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pha Analytical, Inc. <br /> 255 Glendale Ave. -Suite 21 •Sparks,Nevada 89431-5778 <br /> A& (775)355-1044 •(775)355-0406 FAX• 1-800-283-1183 <br /> Date: Q ry p C Summa Report Work Order: <br /> 04-Au¢-09 09072252 <br /> Method Blank Type MBLK Test Code: EPA Method SW60201 SW6020A <br /> File ID: 072909.Bk028SMPL.Dk Batch ID:22416 Analysis Date: 07/291200914:05 <br /> Sample ID: MB-22416 Units: pg/Kg Run ID:ICPIMS_090729A Prep Date: 07128/2009 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> Lead(Pb) ND 1000 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW6020 I SW6020A <br /> File ID:072909.Bk029 LCS.Dk Batch ID:22416 Analysis Date: 07/2912009 14:11 <br /> Sample ID: LCS-22416 Units : pg/Kg Run ID:ICPIMS_090729A Prep Date: 07/28/2009 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> Lead(Pb) 23600 1000 25000 94 80 122 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW6020/SW6020A <br /> File ID: 072909.Bk033SMPL.Dk Batch ID:22416 Analysis Date: 07/29/2009 14:34 <br /> Sample ID: 09072156-01AMS Units: lig/Kg Run ID:ICPIMS_090729A Prep Date: 07128/2009 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> Lead(Pb) 26300 1000 25000 5731 82 68 141 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW6020/SW6020A <br /> File ID: 072909.Bk034SMPL.Dk Batch ID:22416 Analysis Date: 07129/2009 14:39 <br /> Sample ID: 09072156.01AMSD Units: jig/Kg Run ID:ICP/MS_090729A Prep Date: 07/2812009 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> Lead(Ph) 27600 1000 25000 5731 87 68 141 26290 4.9(20) <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br /> Reported in micrograms per Kilogram,per client request. <br />