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alpha Analytical, Inc. .� <br /> 255 Glendale Ave. • Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044 •(775)355-0406 FAX• 1-800-283-1183 <br /> Date: <br /> l- QC Summary Report Work Order: <br /> 28-Jul-09 09072252 <br /> Method Blank Type MBLK Test Code: EPA Method SW8015B <br /> File ID:09072307.D Batch ID:MSISS2381B Analysis Date: 07/23/200910:48 <br /> Sample ID: MBLK MSlSS2381 B Units: pg/Kg Run ID:MSD_15_090723A Prep Date: 07/23/2009 <br /> Analyte Result POL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> TPH-P(GRO) ND 1000 <br /> Surr: 1,2-Dichloroethane-d4 197 200 98 70 130 <br /> Surr:Toluene-d8 204 200 102 70 130 <br /> Surr:4-Bromofluorobenzene 197 200 99 70 130 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8015B <br /> File ID: 09072310.D Batch ID:MS15S2381B Analysis Date: 07/23/2009 11:55 <br /> Sample ID: GLCS MSlSS2381B Units: pg/Kg Run ID:MSD_15_090723A Prep Date: 07/23/2009 <br /> Analyte Result PCL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> TPH-P(GRO) 14500 2000 16000 90 70 139 <br /> Surr: 1,2-Dichloroethane-d4 415 400 104 70 130 <br /> Surr:Toluene-d8 383 400 96 70 130 <br /> Surr:4-Bromofluorobenzene 384 400 96 70 130 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8015B <br /> File ID:09072313.D Batch ID:MS15S2381 B Analysis Date: 07/23/2009 13:02 <br /> Sample ID: 09072120-01AGS Units: pg/Kg Run ID:MSD_15_090723A Prep Date: 07/23/2009 <br /> Analyte Result POL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> TPH-P(GRO) 16100 2000 16000 0 101 57 147 <br /> Surr: 1,2-Dichloroethane-d4 398 400 99 70 130 <br /> Surr:Toluene-d8 390 400 98 70 130 <br /> Surr:4-Bromofluorobenzene 390 400 98 70 130 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8015B <br /> File ID:09072314.D Batch ID: MSISS2381B Analysis Date: 07/23/2009 13:24 <br /> Sample ID: 09072120-01AGSD Units:pg/Kg Run 10:MSD 15090723A Prep Date: 07/23/2009 <br /> Analyle Result POL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> TPH-P(GRO) 15300 2000 16000 0 95 57 147 16120 5.4(20) <br /> Surr: 1,2-Dichloroethane-d4 395 400 99 70 130 <br /> Surr: Toluene-d8 395 400 99 70 130 <br /> Surr: 4-Bromofluorobenzene 386 400 97 70 130 <br /> Comments: <br /> Calculations arc based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br /> Reported in micrograms per Kilogram,per client request. <br />