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(_alpha Analytical, Inc. U <br /> Q 255 Glendale Ave. •Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044 •(775)355-0406 FAX • 1-800-283-1183 <br /> Date: work Order: <br /> 28-Jul-09 QC Summary Report 090722" <br /> Method Blank Type MBLK Test Code: EPA Method SW8260B <br /> File ID:09072307.D Batch ID:MSISS2381A Analysis Date: 07/23/2009 10:48 <br /> Sample ID: MBLK MS15S2381A Units: pg/Kg Run ID:MSD 15090723A Prep Dale: 07/23/2009 <br /> Analyte Result PQL SpkVal SpkRefVal %REG LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> Methyl tert-butyl ether(MTBE) ND 5 '.. <br /> Benzene ,. NO 5 <br /> Toluene NO 5 <br /> Ethylbenzene ND 5 <br /> m,p-XVlene ND 5 <br /> o-XVlene - ND 5 - a <br /> Surr: 1,2-Dichloroethane-d4 197 200 98 70 130 .I <br /> Surr Toluene-d8 204 200 102 70 130 <br /> Surr:4-Bromofluorobenzene 197 200 99 70 130 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8260B <br /> File ID:09072309.D Batch ID:MSISS2381A Analysis Date: 07/23/2009 11:33 <br /> Sample ID: LCS MSlSS2381A Units: pg/Kg _ Run ID:MSD_15_090723A Prep Date: 07/23/2009 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> Methyl ten-butyl ether(MTBE) 442 10 400 111 65 144 <br /> Benzene 415 10 400 104 70 136 <br /> Toluene 376 10 400 94 70 135 <br /> Ethylbenzene 391 10 400 98 70 137 <br /> m,p-Xylene 411 10 400 - 103 70 143 <br /> o-XVlene 415 10 400 _ 104 70 143 <br /> Surr: 1,2-Dichloroethane-d4 392 400 98 70 130 <br /> Surr Toluene-d8 385 - 400 96 70 130 <br /> Surr: 4-Bromofluorobenzene 387 400 97 70 130 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW82608 <br /> File ID: 09072311.0 Batch ID:MS15152381A Analysis Date: 07/23/2009 12:17 <br /> Sample ID: 09072120-01AMS Units : pg/Kg Run ID:MSD_15_090723A Prep Date: 07/23/2009 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> Methyl tert-butyl ether(MTBE) 468 10 400 0 117 42 156 <br /> Benzene 429 10 400 0 107 57 143 <br /> Toluene 389 10 400 t' 0 97 53 142 <br /> Ethvlbenzene 399 10 400 0 99.7 56 145 <br /> m,p-XVlene 428 10 400 0 107 53 154 <br /> o-XVlene 433 10 400 0 108 60 148 <br /> Surr: 1,2-Dichloroethane-d4 394 400 - 99 70 130 <br /> Surr:Toluene-d8 378 400 95 70 130 <br /> Surr:4-Bromofluorobenzene 395 400 99 70 130 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8260B <br /> File ID:09072312.D Batch ID:MS15S2381A Analysis Date: 07/23/200912:39 <br /> Sample ID: 09072120-01AMSO Units: pg/Kg Run ID:MSO_15_090723A Prep Date: 07/23/2009 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> Methyl tert-butyl ether(MTBE) 423 10 400 0 106 42 156 467.6 10.1(20) <br /> Benzene 413 10 400 0 103 57 143 429.4 4.0(20) <br /> Toluene 379 10 400 0 95 53 142 388.6 2.6(20) <br /> Ethylbenzene 396 10 400 0 99 56 145 399 0.9(20) <br /> m,p-Xylene 416 10 400 0 104 53 154 427.7 2.8(20) <br /> o-Xylene 418 10 400 0 105 60 148 433.4 3.5(20) <br /> Surr: 1,2-Dichloroethane-d4 389 400 97 70 130 <br /> Surr:Toluene-d8 - 389 400 97 70 130 <br /> Surr:4-Bromofluorobenzene 392 400 - 98 70 130 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data. However,for reporting purposes,all QCdata is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br /> 1 <br /> I <br />