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BSKLABOR..A.-TORIES <br /> AMENDED REPORT <br /> Nick Berzins Certificate of Analysis , <br /> Tn-Hydra ELAP Certificate#1180 <br /> 4081 E. La Palma Suite A Report Issue Date 12/02/2003 <br /> Anaheim, CA 92807 <br /> BSK Submission#: 2003101529 <br /> BSK Sample ID#• 382151 <br /> Project ID 350-006-003 Project Desc <br /> Submission Comments <br /> Sample Type Solid Date Sampled 10/21/2003 ' <br /> Sample Descnptton UST Bi-1 Time Sampled 1024 <br /> Sample Comments Date Received 10/23/2003 <br /> Organics Analysis <br /> , <br /> Prep Y <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPH as Gasoline EPA 8015(M) ND mg/Kg I 1 1 10/29/03 10/29/03 <br /> 1,2-Dtbromoethane EPA 8260 ND 118/K9 5 0 1 5 10/27/03 10/28/03 <br /> 1,2-Dtchloroethane EPA 8260 ND R&%s 50 1 5 10/27/03 10/28/03 <br /> Eh-isopropyl Ether EPA 8260 ND pglKg 50 1 5 10/27/03 10/28/03 <br /> Ethyl t-Butyl Ether EPA 8260 ND gg/Kg 50 1 5 10/27/03 10/28/03 <br /> Methyl-t-Butyl Ether EPA 8260 ND µ$/Kg 50 1 5 10/27/03 10/28/03 <br /> t-Amyl Methyl Ether EPA 8260 ND A9(Kg 5 0 1 5 10/27/03 10/28/03 <br /> ted-Butyl Alcohol EPA 8260 ND Ng/Kg 50 1 50 10/27/03 10/28/03 <br /> Benzene EPA 8260/5030 ND pg/K8 5 0 1 5 11/04/03 11/04/03 <br /> Ethylbenzene EPA 8260/5030 ND µg/Kg 50 1 5 11/04/03 11/04/03 <br /> m,p-Xylenes EPA 8260/5030 ND µg%g 50 1 5 11/04/03 11/04/03 <br /> o-Xylene EPA 8260/5030 ND pg/Kg 5 0 1 5 11/04103 11/04/03 <br /> Toluene EPA 8260/5030 ND µg/Kg 50 1 5 11/04/03 11/04/03 <br /> Total Xylene Isomers EPA 8260/5030 ND R9/4 50 1 5 11/04/03 11/04103 <br /> Surrogate , <br /> ____________ ___-------- <br /> /o G _ <br /> Fluorobenzene EPA 8015(M) 71,2 Rec 1 N/A 10/29/03 10/29/03 <br /> Toluene-d8 EPA 8260 92 %Rec I N/A 10/27/03 10/28/03 <br /> Bromofluorobenzene EPA 8260/5030 95 %Ret I NIA 11/04/03 11/04/03 , <br /> Dibromofluoromethane EPA 8260/5030 100 %Rec 1 NIA 11/04/03 11/04/03 <br /> Toluene-d8 EPA 8260/5030 92 %Ret 1 NIA 11/04/03 11/04/03 <br /> mg/L MtlhgramslUter(ppm) PQL Practical Quantitation Limit H Analyzed outside of hold time <br /> mg/Kg Milltgmms/Kilogram(ppm) DLR Detection Limit for Reporting P Preliminary result ' <br /> pg/L MtcrogramsfUter(ppb) PQL x Dilution S Suspect result See Cover Letter for comments <br /> pg/Kg Micrograms/Kilogram(ppb) ND None Detected at DLR E Analysis performed by External laboratory <br /> %Rec Percent Recovered(surrogates) See External Laboratory Report attachments <br /> Report Authentication Code 1111111l 1111111111 11111K Page 1 of 6 , <br /> 1414 Stanislaus Street Fresno CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />