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BSKANALYTICAL <br /> LABORATORIES <br /> AMENDED REPORT <br /> rNick Berzlns Certificate of Analysis <br /> Tn-Hydro ELAP Certificate#1'1184 <br /> 1 4081 E La Palma Sti.lte A Report Issue Date 12/02/2003 <br /> Anaheim, CA 92807 <br /> BSK Submission#- 2003101529 <br /> BSK Sample ID# 382152 <br /> ProjeetlD 350-006-003 Project Desc <br /> Submission Comments <br /> Sample Type Solid Date Sampled 10/2112003 <br /> Sample Description UST B 1-2 Time Sampled 1027 <br /> ' Sample Comments Date Received 10/23/2003 <br /> Organics Prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> ' TPH as Gasoline EPA 8015(M) ND mg/Kg 1 1 1 10/29/03 10/29/03 <br /> 1,2-Dtbromoethane EPA 8260 ND pg/Kg 50 1 5 10/27/03 10/28/03 <br /> 1,2-Dtchloroethanc EPA 8260 ND pg/Kg 50 1 5 10/27/03 10/28/03 <br /> I Dr-isopropyl Ether EPA 8260 ND pg/Kg 50 1 5 10/27/03 10/28/03 <br /> Ethyl t-Butyl Ether EPA 8260 ND up/Kg 5 0 1 5 10127103 10/28/03 <br /> Methyl-t-Butyl Ether EPA 8260 ND pg/Kg 50 1 5 10/27/03 10/28/03 <br /> t-Amyl Methyl Ether EPA 8260 ND pg/Kg 50 1 5 10/27/03 10/28/03 <br /> tent-Butyl Alcohol EPA 8260 ND pg/Kg 50 1 50 10/27/03 10128/03 <br /> Benzene EPA 8260/5030 ND pg/Kg 50 1 5 11/04/03 11/04/03 <br /> Dtchlorodtiluommethane EPA 8260/5030 ND pg/Kg 5 0 1 5 11/04/03 11/04/03 <br /> ' Ethylbenzene EPA 8260/5030 ND gg/Kg 50 1 5 11/04/03 11/04/03 <br /> m,p-Xylenes EPA 8260/5030 ND pg/Kg 50 1 5 11/04/03 11/04/03 <br /> o-xylene EPA 8260/5030 ND pg/Kg 50 1 5 11/04/03 11/04/03 <br /> Toluene EPA 8260/5030 ND pg/Kg 50 1 5 11/04/03 11/04/03 <br /> Total Xylene isomers EPA 8260/5030 ND }Ag/Kg 50 1 5 11/04/03 11/04/03 <br /> Surrogate <br /> Fluombenzene EPA 8015(M) 998 /o Rec I NIA 10/29/03 10/29/03 <br /> Toluene-08 EPA 8260 94 %Rec 1 NIA 10127103 10/28/03 <br /> BromD(lu0robenzene EPA 8260/5030 89 %Rec I N/A 11/04/03 11/04/03 <br /> Dhbromofluoromethane EPA 8260/5030 99 %Rec I NIA 11/04/03 11/04/03 <br /> Toluen"8 EPA 8260/5030 92 %Rec 1 N/A i]/04/03 11/04/03 <br /> ' mg/L Milligrams/Liter(ppm) PQL Practical Quantitation Limit H Analyzed outside of hold time <br /> mg/Kg Milligrams/Kilogram(ppm) DLR Detection Limit for Reporting P Preliminary result <br /> pgfL Micrograms/Liter(ppb) PQL x Dilution S Suspect result See Cover Letter for comments <br /> ' pg/Kg Micrograms/Kilogram(ppb) ND None Detected at DLR E Analysts performed by External laboratory <br /> %Rec Percent Recovered(surrogates) See External Laboratory Report attachments <br /> Report MtbanncateonCode 1111111111111111111111111111111111111111111111111IM111111111111U111111IU111g1 Page 2 of 6 <br /> 1414 Stanrslaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559485-6935 <br />