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Alpha Analytical, Inc. 255 Glendale Ave - Suite 21 • Sparks,Nevada 89431-5778 0 4& (775)355-I044- (775)355-0406 FAX• 1-800-283-1183 Date 28-May-04 QC Summary Report Work Order 04051845 Method Blank Type MBLK Test Code EPA Method SW8015 File ID C 1DXIAATA14a052101 d54 Batch ID 9985 Analysis Date 05/22/2004 18 39 Sample ID MBLK-9985 Units pg/L Run ID FID 4_040525A Prep Date 05/22/2004 Analyte Result PQL SpkVal SpkRefVat %REC Lowt.imit HighLimit RPDRefVal %RPD(Limit) Qual TPH-E(Diesel) ND 50 Surr Nonane 104000 100000 104 40 155 Laboratory Control Spike Type LCS Test Code EPA Method SW8015 File ID C IDXIDATA\4ao52101 d55 Batch ID 9985 Analysis Date 05/22/2004 19 12 Sample ID LCS-9985 Units pg/L Run ID FID 4_040525A Prep Date 05/22/2004 Analyte Result PQL SpkVal SpkRefVal %REC LowLimlt HighLimit RPDRefVal %RPD(Limit) Qua] TPN-E (Diesel) 1920 50 2500 77 57 135 Surr Nonane 91800 100000 92 40 135 Sample Matrix Spike Type MS Test Code EPA Method SW8015 File ID C IDXIDATA14a052101 d77 Batch ID 9985 Analysis Date 05/23/2004 07 17 Sample ID 04051845-37AMS Units pg/L Run ID FID 4 040525A Prep Date 05/22/2004 Anatyte Result PQL SpkVal SpkRefVal %REC Lowt-imlt Hightimit RPDRefVal %RPD(Limit) Qual TPH-E(Diesel) 3290 50 2500 0 131 57 162 Surr Nonane 129000 100000 129 40 155 Sample Matnx Spike Duplicate Type MSD Test Code EPA Method SW8015 File ID C 1DXIDATA14ao52101 d78 Batch ID 9985 Analysis Date 05/23/2004 07 51 Sample ID 04051845-37AMSD Units pg/L Run ID FID 4 040525A Prep Date 05/22/2004 alyte Result PQL SpkVal SpkRefVal %REC Lowl-emit HighLimit RPDRefVal %RPD(Limit) Qua] H-E(Diesel) 2900 50 2500 0 116 57 162 3285 12 5(60) Surr Nonane 118000 100000 118 40 155 Comments Calculations are based off of raw(non rounded)data However,for reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated values may differ slightly Reported in micrograms per liter,per client request