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Alpha Analytical, Inc. 255 Glendale Ave - Suite 21 -Sparks,Nevada 89431-5778 0 4& (775)355-1044- (775)355-0406 FAX- 1-800-283-1183 Date Work Order- 28-May-04 QC Summary Report 04051845 Method Blank Type MSLK Test Code EPA Method SW8015 File ID Batch ID 9986 Analysis Date 05/23/2004 02 46 Sample ID MBLK 9986 Units lig/L Run ID FID_1 040522C Prep Date 05/23/2004 Analyte Result PQL SpkVal SpkRefVal %AEC Lowl imit HighLimtt RPDRefVal %RPD(Limrt) Qual TPH-E(Diesel) ND 50 Surr Nonane 94300 100000 94 40 155 Laboratory Control Spike Type LCS Test Code EPA Method SW8015 File ID Batch ID 9986 Analysis Date 05/23/2004 03 16 Sample ID LCS_9986 Units pg/L Run ID FID_1_040522C Prep Date 05/23/2004 Analyte Result PQL SpkVal SpkRefVal %REC LowL.imit HighLimit RPDRefVal %RPD(Limit) Qual TPH-E(Diesel) 2780 500 2500 111 57 135 Surr Nonane 88700 100000 89 40 135 Sample Matrix Spike Type MS Test Code EPA Method SW8015 File ID Batch ID 9986 Analysis Date 05/26/2004 17 13 Sample ID 04052203-01AMS Units pg/L Run ID FID 1_040522C Prep Date 05/22/2004 Analyte Result PQL SpkVal SpkRefVal %REC LowLimd HighUrnit RPDRefVal %RPD(Limit) Qual TPH-E (Diesel) 2570 500 2500 0 103 57 162 Surr Nonane 75100 100000 75 40 155 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW80i5 File ID Batch I 9986 Analysis Date 05/26/2004 17 44 Sample ID 04052203-01AMSD Units pg/L Run ID FID_1_040522C Prep Date 05/22/2004 AftaIyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Dual "ITPH-E(Diesel) 2680 500 2500 0 107 57 162 2567 4 2(60) Surr Nonane 73200 100000 73 40 155 Comments Calculations are based off of raw(non-rounded)data However,for reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated values may differ slightly Reported in micrograms per liter,per client request I •