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Alpha Analytical, Inc. <br /> 255 Glendale Ave •Suite 21 •Sparks,Nevada 89431-5778 <br /> 4& (775)355-I044 • (775)355-0406 FAX• 1-800-283-1183 <br /> IsDate <br /> 28-May-oa QC Summary Report Woo ss s <br /> Method Blank Type MBLK Test Code EPA Method SW8015B/DHS LUFC Manual <br /> File ID D 1HPCHEM\MS091DATA\040519104051940 D Batch ID MS09S99428 Analysis Date 05/19/2004 22 34 <br /> Sample ID MBLK MS09S9942B Units pg/Kg Run ID MSD_09 040519B Prep Date 05/19/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimd Highl-emit RPDRefVal %RPD(Limit) Qual <br /> TPH Purqeable ND 1000 <br /> Surr 1,2-Dichloroethane-d4 208 200 104 70 120 <br /> Surr Toluene-d8 196 200 98 79 124 <br /> Surr 4-Bromofluorobenzene 204 200 102 75 122 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8015B/DHS LUFT Manual <br /> File ID D1HPCHEM1MS091DATA1040519104051942 D Batch ID MS09SS9428 Analysis Date 05/19/20042318 <br /> Sample ID GLCS MS09S9942B Units pg/Kg Run 10 MSD_09 040519B Prep Date 05/19/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Highl-imtt RPDRefVal %RPD(Limit) Qual <br /> TPH Purqeable 9060 1000 8000 113 53 143 <br /> Surr 1,2-Dichloroethane-d4 214 200 107 70 120 <br /> Surr Toluene-d8 198 200 99 79 124 <br /> Surr 4-Bromofluorobenzene 202 200 101 75 122 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8015B/DHS LUFr Manual <br /> File 1D D\HPCHEMIMS091DATA1040519104o51945 D Batch ID MS09S994213 Analysis Date 05/20/2004 00 26 <br /> Sample ID 04051824-01AGS Units jig/Kg Run ID MSD 09_0405198 Prep Date 05/20/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowUmit HighLtmit RPDRefVal %RPD(Limit) Qual <br /> TPH Purqeable 12900 1000 8000 0 161 0 334 <br /> Surr 1,2-Dichloroethane-d4 209 200 105 70 120 <br /> urr Toluene-d8 197 200 99 79 124 <br /> r 4-Bromofluorobenzene 198 200 99 75 122 <br /> NW <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW80158/DHS LOFT Manual <br /> File 0 D\HPCHEM1MS091DATA1040519104051946 D Batch ID MS09S9942B Analysis Date 05/20/2004 00 49 <br /> Sample ID 04051824-01AGSD Units pg/Kg Run ID MSD_09 040519B Prep Date 05/20/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imrt Highl-imit RPDRefVal %RPD(Umit) Qual <br /> TPH Purqeable 13600 1000 8000 0 170 0 334 12910 5 4(88) <br /> Surr 1,2-Dichloroethane-d4 203 200 101 70 120 <br /> Surr Toluene-d8 200 200 100 79 124 <br /> Surr 4-Bromofluorobenzene 197 200 98 75 122 <br /> Comments <br /> Calculations are based off of raw(non-rounded)data However,for reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated <br /> values may differ slightly <br /> Reported in micrograms per kilogram,per client request <br /> 0 <br />