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Alpha Analytical, Inc. 255 Glendale Ave • Suite 21 • Sparks,Nevada 89431-5778 •Date (775)355-1044• (775)355-0406 FAX• 1-800-283-1183 28-May-04 QC Summary Report Work Order 04051845 Method Blank Type MBLK Test Code EPA Method SW8015 File ID C IDXIDATA13a052101 d39 Batch ID 9983 Analysis Date 05/22/2004 15 14 Sample ID MBLK-9983 Units jig/Kg Run ID FID 3_040525A Prep Date 05/22/2004 Analyte Result PQL SpkVal SpkRefVal %REC LowLimd HrghL.imrt RPDRefVal %RPD(Limit) Qual TPH-E(Diesel) ND 1000 Surr Nonane 102000 100000 102 56 148 Laboratory Control Spike Type LCS Test Code EPA Method SW8015 File ID C IDXIDATA13a052101 d37 Batch ID 9983 Analysis Date 05/22/2004 14 11 Sample ID LCs-9983 Units pg/Kg Run ID FID_3 040525A Prep Date 05/22/2004 Analyte Result PQL SpkVal SpkRefVal %REC LowL.imit Highl.imd RPDRefVal %RPD(Limit) Qual TPH-E(Diesel) 102000 1000 100000 102 44 148 Surr Nonane 114000 100000 114 56 148 Sample Matnx Spike Type MS Test Code EPA Method SW8015 File ID C\DX\DATA13a052101 d63 Batch ID 9983 Analysis Date 05/23/2004 04 07 Sample ID 04051845-44AMS Units pg/Kg Run ID FID_3_040525A Prep Date 05/22/2004 Analyte Result PQL SpkVal SpkRefVal %REC Lowtimit Highi-imit RPDRefVal %RPD(Umit) Qual TPH-E(Diesel) 95400 1000 100000 0 95 44 153 Surr Nonane 98300 100000 98 56 148 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8015 File ID C 1DXDATA13a052101 d64 Batch ID 9983 Analysis Date 05/23/2004 D4 39 Sample 1D 04051845-44AMSD Units pg/Kg Run ID FID_3_040525A Prep Date 05/22/2004 AlIkalyte Result PQL SpkVal SpkRefVal %REC LowLimit Hlghl-imit RPDRefVal %RPD(Limit) Qual H-E(Diesel) 94000 1000 100000 0 94 44 153 95350 1 4(49) Surr Nonane 93900 100000 94 56 148 Comments Calculations are based off of raw(non-rounded)data However,for reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated values may differ slightly Reported in micrograms per kilogram,per client request I