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Alpha Analytical, Inc. 255 Glendale Ave • Suite 21 •Sparks,Nevada 89431-5778 (775)355-1044- (775)355-0406 FAX• 1-800-283-1183 •Date 28 May-04 QC Summary Report Work Order 04051845 Method Blank Type MBLK Test Code EPA Method SW8015 File 1D C N=DATA13a052101 d40 Batch ID 9984 Analysts Date 05/22/2004 15 46 Sample ID MBLK-9984 Units pg/Kg Run ID FID 3 040525A Prep Date 05/22/2004 Analyte Result POL SpkVai SpkRefVal %REC LOwLimlt HighUrnit RPDRefVal %RPD(Lamit) Qual TPH-E (Diesel) ND 1000 Surr Nonane 119000 100000 119 56 148 Laboratory Control Spike Type LCS Test Code EPA Method SW8015 File ID C%DXIDATA13a052101 d3e Batch ID 9984 Analysis Date 05/22/2004 14 43 Sample ID LCS-9984 Units pg/Kg Run ID FID_3_040525A Prep Date 05/22/2004 Analyte Result PQL SpkVai SpkRefVal %REC Lowl-imit Highl-imit RPDRefVal %RPD(Umit) Qual TPH-E(Diesel) 97900 1000 100000 98 44 148 Surr Nonane 103000 100000 103 56 148 Sample Matrix Spike Type MS Test Code EPA Method SW8015 File ID C 1DX\DATA13a052101 d82 Batch 1D 9984 Analysis Date 05/23/2004 14 26 Sample ID 04052202-04AMS Units pg/Kg Run ID FID3_040525A Prep Date 05/22/2004 Analyte Result PQL SpkVai SpkRefVal %REC Lowl-imit Highl imit RPDRefVal %RPD(Limit) Qual TPH-E(Diesel) 103000 1000 100000 0 103 44 153 Surr Nonane 148000 100000 148 56 148 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8015 File ID C 1DX�DATA13aos2101 d83 Batch ID 9984 Analysis Date 05/23/2004 14 58 Sample ID 04052202-04AMSD Units pg/Kg Run lD FID 3_040525A Prep Date 05/22/2004 Aftalyte Result PQL SpkVai SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual H-E (Diesel) 102000 1000 100000 0 102 44 153 102600 0 1(49) Surr Nonane 148000 100000 148 56 148 Comments Calculations are based off of raw(non-rounded)data However,for reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated values may differ slightly Reported in micrograms per kilogram,per chest request I I