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LancasterReport <br /> Laboratories analysis p <br /> 2425 New Holland Pike PO Box 12425 Lancaster PA 17605.2425 717-656 2300 Fax 717 6565-2681•www lancasterlabs com <br /> Page 3 of 9 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 877375 <br /> Reported 12/23/03 at 02 19 PM <br /> Sample Matrix Quality Control <br /> MS MSD MS/MSD RPA BAf3 DVP DVP Dup <br /> RPD <br /> Analysis Name RSC %REC Limits RPD MAX Conc Conc RPD Max <br /> Batch number 03343A16A Sample number(s) 4177762-4177771 <br /> TPH-GRO - Waters 119 63-154 <br /> Batch number P033431AA Sample number(s) 417773B,4177770-4177771 <br /> Ethanol 112 118 38-149 5 30 <br /> Methyl Tertiary Butyl Ether 95 95 69-134 1 30 <br /> ds-Isopropyl ether 98 98 75-130 0 30 <br /> Ethyl t-butyl ether 97 98 78-119 1 30 <br /> t-Amyl methyl ether 95 94 77-117 1 30 <br /> t-Butyl alcohol 111 108 44-150 3 30 <br /> Benzene 97 96 83-126 0 30 <br /> Toluene 97 99 83-127 1 30 <br /> Ethylbenzene 99 100 82-129 1 30 <br /> Xylene (Total) 98 98 82-130 1 30 <br /> Batch number P033432AA Sample number(s} 4177746-4177754 <br /> Ethanol 144 134 38-149 7 30 <br /> Methyl Tertiary Butyl Ether 91 90 69-134 1 30 <br /> di-Isopropyl ether 96 95 75-130 1 30 <br /> Ethyl t-butyl ether 95 94 78-119 1 30 <br /> t-Amyl methyl ether 94 91 77-117 2 30 <br /> t-Butyl alcohol 109 107 44-150 2 30 <br /> Benzene 97 96 83-128 2 30 <br /> Toluene 98 98 83-127 0 30 <br /> Ethylbenzene 96 96 82-129 1 30 <br /> Xylene (Total) 96 95 82-130 0 30 <br /> Batch number P033441AA Sample number(s) 4177733-4177737,4177739-4177744,4177755-4177757 <br /> Ethanol 133 120 38-149 11 30 <br /> Methyl Tertiary Butyl Ether 90 87 69-134 3 30 <br /> di-Isopropyl ether 95 94 75-130 2 30 <br /> Ethyl t-butyl ether 96 93 78-119 3 30 <br /> t-Amyl methyl ether 95 93 77-117 2 30 <br /> t-Butyl alcohol 117 118 44-150 1 30 <br /> Benzene 94 93 83-128 1 30 <br /> Toluene 95 92 83-127 3 30 <br /> Ethylbenzene 98 96 82-129 3 30 <br /> Xylene (Total) 98 96 82-130 2 30 <br /> Batch number P033442AA Sample number(s) 4177745,4177758-4177765 <br /> Ethanol 143 149 3B-149 4 30 <br /> Methyl Tertiary Butyl Ether 91 91 69-134 0 30 <br /> di-Isopropyl ether 95 97 75-130 2 30 <br /> Ethyl t-butyl ether 95 96 78-119 1 30 <br /> t-Amyl methyl ether 92 95 77-117 3 30 <br /> t-Butyl alcohol 110 110 44-150 0 30 <br /> Benzene 94 97 83-128 3 30 <br /> Toluene 96 98 83-127 2 30 <br /> Ethylbenzene 95 96 82-129 1 30 <br /> Xylene {Total) 95 97 82-130 1 30 <br /> Batch number P033451AA Sample number(s) 4177766-4177769 <br /> Ethanol 122 128 38-149 5 30 <br /> Methyl Tertiary Butyl Ether 93 90 69-134 3 30 <br /> *-Outside of specification <br /> (l) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the spike added <br />