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Lancaster <br /> f1p Laboratories Analysis Report <br /> 2425 New Holland Pike PO Box 12425 Lancaster PA 17605-2425•717 656 2300 Fax 717-656-2681•www lancastedabs corn <br /> Page 4 of 9 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 877375 <br /> Reported 12/23/03 at 02 19 PM <br /> Sample Matrix Quality Control <br /> Ms MSD MS/MSD RPD ERG DUP DUP Dup <br /> RPD <br /> Analvais Name %REC %REC Limits RPD MAX Conc Conc RPA Max- <br /> di-Isopropyl ether 96 94 75-130 2 30 <br /> Ethyl t-butyl ether 94 93 78-119 1 30 <br /> t-Amyl methyl ether 94 93 77-117 1 30 <br /> t-Butyl alcohol 119 118 44-150 0 30 <br /> Benzene 95 93 83-128 2 30 <br /> Toluene 96 95 83-127 1 30 <br /> Ethylbenzene 98 96 82-129 1 30 <br /> Xylene (Total) 97 96 82-130 1 30 <br /> Batch number W033462AA Sample number(s) 4177732 <br /> Methyl Tertiary Butyl Ether 102 69-134 <br /> Benzene 103 83-128 <br /> Toluene 102 83-127 <br /> Ethylbenzene 102 82-129 <br /> Xylene (Total) 101 82-130 <br /> Surrogate Quality Control <br /> Analysis Name TPH - DRO CA LUST (Waters) <br /> 0 Batch number 033400010A <br /> Orthoterphenyl <br /> 4177741 135 <br /> 4177744 90 <br /> 4177745 89 <br /> 4177746 94 <br /> 4177747 95 <br /> 4177748 135 <br /> 4177749 0* <br /> 4177750 0* <br /> 4177752 834* <br /> 4177753 120 <br /> 4177755 88 <br /> 4177757 82 <br /> 4177758 78 <br /> 4177759 89 <br /> Blank B7 <br /> LCS 93 <br /> LCSD 91 <br /> I <br /> Limits 59-139 <br /> Analysis Name TPH - DRO CA LUFT (Waters) <br /> Batch number G33400014A <br /> Orthoterphenyl <br /> 4177733 133 <br /> 4177734 79 <br /> 4177735 105 <br /> 4177736 154* <br /> 4177737 83 <br /> 4177738 290" <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the spike added <br /> I <br />