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ANAMETRIX, INC. <br /> 1961 CONCOURSE DRIVE, SUITE E <br /> SAN JOSE, CA 95131, (408) 432-8192 <br /> INDIVIDUAL-METALS-MATRIX-SPIKE-REPORT---- <br /> ----- <br />' Spike I.D. 9112187-12MS,MD Inst. ID: AA2 <br /> Date Prepared: 12/23/91 Date : 01/02/92 <br /> Date Analyzed: 12/26/91 Matrix : WATER <br /> Assoc. WO # : 9112187 Units : ug/L <br />' ---------------------------------------------------------------------------- <br /> ELEMENTS METHOD SPIKE SAMPLE M. S. $ M.S.D. % R P D <br /> AMOUNT CONC. * CONC. REC. CONC. REC. <br /> ------------------------------------------------------------------------------ <br /> Pb 239.2 500 5. 3 516 102 531 105 2 .9 <br /> COMMENT: Quality control limits for percent recovery are 75-125% and 25% <br /> for RPD. <br /> * Sample concentration of 0. 0 indicates that the analyte in the <br /> sample was below detection limit for the method. 0. 0 is entered <br /> for calculations of the percent recovery and RPD only. <br />■ <br />■ <br />■ <br />■ <br />■ <br />■ <br /> 1- <br /> Supervi [Date Chemist Date <br />' METALS/METALS - PAGE 5 <br />■ <br />