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r <br /> ANAMETRIX, INC. <br /> 1961 CONCOURSE DRIVE, SUITE E <br /> SAN JOSE, CA 95131, (408) 432-8192 <br /> -------------------------------------------- <br /> INDIVIDUAL <br /> _METALS-MATRIX <br /> -SPIKE-REPORT <br /> ' Spike I.D. 9112187-02MS,MD Inst. ID: AA2 <br /> Date Prepared: 12/23/91 Date : 01/02/92 <br /> Date Analyzed: 12/30/91 Matrix : SOIL <br /> Assoc. WO # : 9112187 Units : mg/Kg <br /> ' ---------------------------------------------------------------------------- <br /> ELEMENTS METHOD SPIKE SAMPLE M.S. -% M.S.D. % R P D <br /> AMOUNT CONC. * CONC. REC. CONC. REC. <br />' ------------------------------------------------------------------------------ <br /> Pb 7421 25. 0 1. 9 27 . 1 101 26. 8 100 1.2 <br /> COMMENT: Quality control limits for percent recovery are 75-125% and 25% <br /> for RPD. <br /> * Sample concentration of 0. 0 indicates that the analyte in the <br /> sample was below detection limit for the method. 0. 0 is entered <br /> far calculations of the percent recovery and RPD only. <br /> ■ <br />■ <br />■ <br />■ <br />■ <br /> Sut'per,Vi 0 1 Date emi Date <br /> I <br />' METALS/METALS - PAGE 6 <br />■ <br />