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QC Sample Results C <br /> Client:Antea USA, Inc. TestAmerica Job ID: 720-56810-1 <br /> Project/Site: UPRR-Stockton <br /> Method: 8260B/CA_LUFTMS - 8260B/CA LUFT MS (Continued) <br /> Lab Sample ID: 720-56810-3 MS Client Sample ID: SO-2432-B-2D5.5-041514 <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 157551 Prep Batch: 157590 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> 1,2,4-Trichlorobenzene ND 0.0452 0.0353 mg/Kg 78 49-144 <br /> 1,1,1-Trichloroethane ND 0.0452 0.0565 mg/Kg 125 57-133 <br /> 1,1,2-Trichloroethane ND 0.0452 0.0468 mg/Kg 103 68-132 <br /> Trichloroethene ND 0.0452 0.0463 mg/Kg 102 66-130 <br /> Trichlorofluoromethane ND 0.0452 0.0575 mg/Kg 127 61-130 <br /> 1,2,3-Trichloropropane ND 0.0452 0.0647 mg/Kg 143 62-150 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha ND 0.0452 0.0498 mg/Kg 110 52-130 <br /> ne <br /> 1,2,4-Trimethylbenzene ND * 0.0452 0.0648 *F1 mg/Kg 143 64-140 <br /> 1,3,5-Trimethylbenzene ND * 0.0452 0.0687 *F1 mg/Kg 152 67-134 <br /> Vinyl acetate ND 0.0452 ND F1 mg/Kg 47 52-150 <br /> Vinyl chloride ND 0.0452 0.0483 mg/Kg 107 62-130 <br /> m-Xylene&p-Xylene ND 0.0904 0.100 mg/Kg 111 70-130 <br /> o-Xylene ND 0.0452 0.0505 mg/Kg 112 68-130 <br /> 2,2-Dichloropropane ND 0.0452 0.0585 mg/Kg 129 63-130 <br /> MS MS El <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene 88 45-131 <br /> 1,2-Dichloroethane-d4(Surr) 110 60-140 <br /> Toluene-d8(Surr) 98 58-140 <br /> Lab Sample ID: 720-56810-3 MSD Client Sample ID: SO-2432-B-2D5.5-041514 <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 157551 Prep Batch: 157590 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Methyl tert-butyl ether ND 0.0482 0.0645 V1 mg/Kg 134 69-130 15 20 <br /> Acetone ND 0.241 0.277 mg/Kg 115 37-150 18 20 <br /> Benzene ND 0.0482 0.0497 mg/Kg 103 70-130 10 20 <br /> Dichlorobromomethane ND 0.0482 0.0572 mg/Kg 119 64-135 8 20 <br /> Bromobenzene ND * 0.0482 0.0683 *F1 F2 mg/Kg 142 70-130 21 20 <br /> Chlorobromomethane ND 0.0482 0.0586 mg/Kg 121 65-130 10 20 <br /> Bromoform ND 0.0482 0.0569 mg/Kg 118 58-132 16 20 <br /> Bromomethane ND 0.0482 0.0575 mg/Kg 119 56-130 16 20 <br /> 2-Butanone(MEK) ND 0.241 0.239 mg/Kg 99 41-150 9 20 <br /> n-Butylbenzene ND * 0.0482 0.0825 *F1 F2 mg/Kg 171 60-145 28 20 <br /> sec-Butylbenzene ND * 0.0482 0.0906 *F1 F2 mg/Kg 188 64-137 34 20 <br /> tert-Butyl benzene ND * 0.0482 0.100 *F1 F2 mg/Kg 208 63-134 35 20 <br /> Carbon disulfide ND 0.0482 0.0433 mg/Kg 90 10-150 11 20 <br /> Carbon tetrachloride ND 0.0482 0.0662 F1 mg/Kg 137 54-130 11 20 <br /> Chlorobenzene ND * 0.0482 0.0517 mg/Kg 107 70-130 12 20 <br /> Chloroethane ND 0.0482 0.0569 mg/Kg 118 61-130 17 20 <br /> Chloroform ND 0.0482 0.0603 mg/Kg 125 67-130 11 20 <br /> Chloromethane ND 0.0482 0.0505 mg/Kg 105 50-131 17 20 <br /> 2-Chlorotoluene ND * 0.0482 0.0820 *F1 F2 mg/Kg 170 70-130 28 20 <br /> 4-Chlorotoluene ND * 0.0482 0.0721 *F1 F2 mg/Kg 150 70-130 23 20 <br /> Chlorodibromomethane ND 0.0482 0.0517 mg/Kg 107 60-141 5 20 <br /> 1,2-Dichlorobenzene ND * 0.0482 0.0491 mg/Kg 102 70-130 9 20 <br /> TestAmerica Pleasanton <br /> Page 141 of 241 4/29/2014 <br />