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QC Sample Results C <br /> Client:Antea USA, Inc. TestAmerica Job ID: 720-56810-1 <br /> Project/Site: UPRR-Stockton <br /> Method: 8260B/CA_LUFTMS - 8260B/CA LOFT MS (Continued) <br /> Lab Sample ID:720-56810-3 MSD Client Sample ID:SO-2432-B-2D5.5-041514 <br /> Matrix: Solid Prep Type:Total/NA <br /> Analysis Batch: 157551 Prep Batch: 157590 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> 1,3-Dichlorobenzene ND 0.0482 0.0584 * mg/Kg 121 70-130 13 20 <br /> 1,4-Dichlorobenzene ND 0.0482 0.0542 * mg/Kg 113 70-130 10 20 <br /> 1,3-Dichloropropane ND 0.0482 0.0503 mg/Kg 104 70-130 7 20 <br /> 1,1-Dichloropropene ND 0.0482 0.0576 mg/Kg 120 67-130 9 20 <br /> 1,2-Dibromo-3-Chloropropane ND 0.0482 0.0567 *F2 mg/Kg 118 57-130 26 20 <br /> Ethylene Dibromide ND 0.0482 0.0491 mg/Kg 102 66-135 5 20 <br /> Dibromomethane ND 0.0482 0.0547 mg/Kg 114 65-131 8 20 <br /> Dichlorodifluoromethane ND 0.0482 0.0516 mg/Kg 107 38-130 13 20 <br /> 1,1-Dichloroethane ND 0.0482 0.0589 mg/Kg 122 67-130 15 20 <br /> 1,2-Dichloroethane ND 0.0482 0.0599 mg/Kg 124 70-130 11 20 <br /> 1,1-Dichloroethene ND 0.0482 0.0551 mg/Kg 114 64-130 12 20 <br /> cis-1,2-Dichloroethene ND 0.0482 0.0555 mg/Kg 115 68-131 10 20 <br /> trans-1,2-Dichloroethene ND 0.0482 0.0541 mg/Kg 112 70-130 12 20 <br /> 1,2-Dichloropropane ND 0.0482 0.0530 mg/Kg 110 65-133 10 20 <br /> cis-1,3-Dichloropropene ND 0.0482 0.0502 mg/Kg 104 46-139 5 20 <br /> trans-1,3-Dichloropropene ND 0.0482 0.0512 mg/Kg 106 55-131 4 20 <br /> Ethylbenzene ND 0.0482 0.0595 mg/Kg 124 65-130 20 20 <br /> Hexachlorobutadiene ND 0.0482 0.0703 *F1 F2 mg/Kg 146 58-132 28 20 <br /> 2-Hexanone ND 0.241 0.248 mg/Kg 103 44-150 12 20 <br /> Isopropylbenzene ND 0.0482 0.0632 F1 mg/Kg 131 65-130 17 20 <br /> 4-Isopropyltoluene ND * 0.0482 0.0913 *F1 F2 mg/Kg 189 69-134 31 20 <br /> Methylene Chloride ND 0.0482 0.0522 mg/Kg 108 63-130 14 20 <br /> 4-Methyl-2-pentanone(MIBK) ND 0.241 0.265 mg/Kg 110 51-140 12 20 <br /> Naphthalene ND 0.0482 0.0186 *F1 F2 mg/Kg 39 45-146 25 20 <br /> N-Propylbenzene ND 0.0482 0.0924 *F1 F2 mg/Kg 192 70-130 35 20 <br /> Styrene ND 0.0482 0.0462 mg/Kg 96 58-135 2 20 <br /> 1,1,1,2-Tetrachloroethane ND 0.0482 0.0734 F1 F2 mg/Kg 152 64-133 22 20 <br /> 1,1,2,2-Tetrachloroethane ND 0.0482 0.0855 *F1 F2 mg/Kg 177 70-131 41 20 <br /> Tetrachloroethene ND 0.0482 0.0529 mg/Kg 110 67-130 3 20 <br /> Toluene ND 0.0482 0.0642 F1 F2 mg/Kg 133 70-130 23 20 <br /> 1,2,3-Trichlorobenzene ND 0.0482 0.0262 *F1 mg/Kg 54 58-138 12 20 <br /> 1,2,4-Trichlorobenzene ND 0.0482 0.0331 * mg/Kg 69 49-144 6 20 <br /> 1,1,1-Trichloroethane ND 0.0482 0.0648 F1 mg/Kg 135 57-133 14 20 <br /> 1,1,2-Trichloroethane ND 0.0482 0.0511 mg/Kg 106 68-132 9 20 <br /> Trichloroethene ND 0.0482 0.0501 mg/Kg 104 66-130 8 20 <br /> Trichlorofluoromethane ND 0.0482 0.0652 F1 mg/Kg 135 61-130 13 20 <br /> 1,2,3-Trichloropropane ND * 0.0482 0.0996 *F1 F2 mg/Kg 207 62-150 42 20 <br /> 1,1,2-Trichloro-1,2,2-trifluoroetha ND 0.0482 0.0566 mg/Kg 117 52-130 13 20 <br /> ne <br /> 1,2,4-Trimethylbenzene ND 0.0482 0.0852 *F1 F2 mg/Kg 177 64-140 27 20 <br /> 1,3,5-Trimethyl benzene ND * 0.0482 0.0942 *F1 F2 mg/Kg 196 67-134 31 20 <br /> Vinyl acetate ND 0.0482 ND F1 F2 mg/Kg 13 52-150 111 20 <br /> Vinyl chloride ND 0.0482 0.0565 mg/Kg 117 62-130 16 20 <br /> m-Xylene&p-Xylene ND 0.0963 0.118 mg/Kg 123 70-130 17 20 <br /> o-Xylene ND 0.0482 0.0586 mg/Kg 122 68-130 15 20 <br /> 2,2-Dichloropropane ND 0.0482 0.0686 F1 mg/Kg 142 63-130 16 20 <br /> TestAmerica Pleasanton <br /> Page 142 of 241 4/29/2014 <br />