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i <br /> GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209)572.0900 Fax(209)572-0916 <br /> WJ- <br /> port# S6D1311 Project: Pombo Ranch-Quarterly Date: 04/20/06 Kloberdanz&Associates Date Rec'd: 04/13/06 <br /> P.O. Box 576981 PO# <br /> Modesto, CA 95357 <br /> Volatile Organic Chemistry of Hazardous Waste- Quality Control <br /> GeoAnalytical Laboratories, Inc. <br /> Reporting Spike Source %REC RPD <br /> LaMe Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch SO01319-EPA 5030B Prepared &Analyzed: 04/14/06 <br /> Blank(S001319-BLK1) <br /> Gasoline NO 0.05 mg/L -----� -----���.--- �- <br /> Surrogate:a,a,a-Tr!uorotoluene 0.0218 0.0150 87 70-125 <br /> LCS(SO413I9-BSl) <br /> Gasoline 0.23 0.05 mg/L 0.250 92 80-120 <br /> Surrogate:a,a,a-Tris luorotoluene 0.0144 0.0150 98 70-125 <br /> Matrix Spike($001319-MSI) -�--_ Source: S6D1311-01 <br /> Gasoline 0.25 0.05 mg/L 0.250 ND 100 51-153 <br /> Surrogate:a,a,a-Trifluorololuene 0.0239 0.0250 Y 96 70-115 <br /> trix Spike Dup(S00__1319-MSD1) -__Source: S6D1311-01 <br /> ohne _ 0.24 _ 0.05 mg/L 0.250 ND 96 51-153 4 25 <br /> Surrogate:a,a,a-Triuorotoluene 0.0243 0.0150 97 70-115 <br /> Batch 5001323 -EPA 5030B Prepared&Analyzed: 04/18/06 <br /> Blank(5001323-BLK_1) <br /> Benzene ND 0.3 ug/i � -- --- <br /> Toluene ND 0.3 " <br /> Ethylbenzene ND 0.3 " <br /> Xylenes,total ND 0.6 " <br /> Methyl tent-Butyl Ether(MTBE) ND 0.5 " <br /> Ethanol ND 40.0 " <br /> tert-Butanol(TBA) ND 5,0 " <br /> Di-isopropyl Ether(DIPE) ND 015 " <br /> Ethyl tert-Butyl Ether(ETBE) ND 0.5 " <br /> Tert-Amyl Methyl Ether(TAME) ND 0,5 " <br /> Ethylene dibromide ND 1.0 " <br /> 1,2-Dichloroethane ND 0.5 " <br /> Surrogate: l,2-Dichloroethane-d4 5.09 ~-� 5.00 102 71-132 - <br /> Surrogate:2-Bromo-l-Chloropropane 4.71 5.00 94 71-134 <br /> Surrogate:4-Bromofluorobenzene 4.89 5.00 98 74-132 <br /> Certification #2585 <br />