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GeoAnalytical Laboratories, Inc. <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone(209)572-0900 Fax(209)572-0916 <br /> port# S6D1311 Project: Pornbo Ranch- Quarterly Date: 04/20/06 <br /> J. Kloberdatlz&Associates Date Rec'd: 04/13/06 <br /> P.O. Box 576981 PON <br /> Modesto,CA 95357 <br /> Volatile Organic Chemistry of Hazardous Waste -Quality Control <br /> GeoAnalytical Laboratories, Inc. <br /> Reporting Spike Source %REC RPD <br /> Lalvte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 5001323-EPA 5030B Prepared & Analyzed: 04/18/06 <br /> LCS(5001323-BSI) <br /> Benzene 9.9 0.3 uglL 10.0 99 80-120 <br /> Toluene 10.7 0.3 10,0 107 80-120 <br /> Methyl tent-Butyl Ether(MTBE) 10.0 0.5 10.0 100 80-120 <br /> Di-isopropyl Ether(DIPS) 9.9 0.5 10.0 99 80-120 <br /> Tert-Amyl Methyl Ether(TAME) 10.1 0.5 10.0 I01 80-120 <br /> 1,2-Dichloroethane 10.2 0.5 10.0 102 80-120 <br /> Surrogate: 1,2-Dichloroethane-d4 5.04 5.00 101 72-132 <br /> Surrogate:2-Bromo-I-Chloropropane 5.09 5.00 102 71-134 <br /> Surrogate.4-Bromofluorobenzene 5.25 5.00 105 74-132 <br /> Matrix Spike(S001323-MSI) Source:S6D0704-01 <br /> 9,uzene 9.2 0.3 ug1L 10.0 ND 92 55-129 <br /> -e-n 10.2 0.3 10.0 ND 102 54-127 <br /> Methyl Cert-Butyl Ether(MTBE) 9.9 0.5 10.0 ND 99 56-150 <br /> Di-isopropyl Ether(DIPS) 9.7 0.5 10.0 ND 97 75-130 <br /> Tert-Amyl Methyl Ether(TAME) 9.8 0.5 10.0 ND 98 67-133 <br /> 1,2-Dichloroethane 9.7 0.5 10.0 ND 97 70-130 <br /> Surrogate: 1,2-Dichloroethane-d4 5.40 5.00 108 72-132 <br /> Surrogate:2-Bromo-l-Chloropropane 5.10 5.00 102 71-134 <br /> Surrogate:4-Bromofluorobenzene 5.05 5.00 101 74-132 <br /> Matrix Spike Dup(S00I323-MSDI)_ _ Source: S6D0704-01____ <br /> Benzene 9.2 0.3 ug/L 10.0 ND 92 55-129 0 21 <br /> Toluene 10.5 03 10.0 ND 105 54-127 3 22 <br /> Methyl Cert-Butyl Ether(MTBE) 8.3 0.5 10.0 ND 83 56-150 18 26 <br /> Di4sopropyl Ether(DIPE) 9.5 0.5 10.0 ND 95 75-130 2 20 <br /> Ten-Amyl Methyl Ether(TAME) 8.8 0.5 10.0 ND 88 67-133 11 21 <br /> 1,2-Dichloroethane 9.0 0.5 10.0 ND 90 70-130 7 20 <br /> Surrogate: 1,2-Dichtoroethane-d4 4.76 5.00 95 72-132 <br /> Surrogate:2-Bromo-l-Chloropropane 4.86 5.00 97 71-134 <br /> Surrogate:4-Bromofluorobenzene 4.80 5.00 96 74-131 <br /> i <br /> I <br /> Certification#2585 <br />