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Entech Analytical Labs, Inc , Santa Clara, CA <br /> Lab Report No H2101009 Date 10/21/2002 Page 3 <br /> 7PrjojectName FRONTIER TRUCKING Analysis Volatile Organic Compounds by GC/MS Fuel <br /> No NA Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW-11 Lab Samp ID 31582-005 <br /> DescrlLocation MW-11 Recd Date 10/11/2002 <br /> Sample Date 10/07/2002 Prep Date 10/13/2002 <br /> Sample Time 1610 Analysis Date 10/13/2002 <br /> Matrix Water QC Batch WMS21748 <br /> Basis Not Filtered Notes <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 03 5 PQL ND UGIL 1 <br /> Ethyl tent-butyl ether(ETBE) 05 5 PQL ND UG1L 1 <br /> tent-Amyl methyl ether(TAME) 03 5 PQL ND UGIL 1 <br /> Di-isopropyl ether(DIPE) 05 5 PQL ND UGIL 1 <br /> tent-Butyl alcohol (TBA) 46 10 PQL ND UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES 1 <br /> 4-Bromofluorobenzene 65-135 SMSA 973% <br /> Toluene-d8 77-150 SMSA 996% 1 <br /> Dibromofluoromethane 57-156 SMEA 1024% 1 <br /> Approved by <br /> Date �_- <br />