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Entech Analytical Labs, Inc , Santa Clara, CA <br /> Lab Report No H2101009 Date 10/21/2002 Page 13 <br /> 7 Project Name FRONTIER TRUCKING Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Protect No NA Method 8260FA <br /> Prep Meth SW5030B <br /> Field ID MW-9 Lab Samp ID 31582-006 <br /> Descr/Location MW-9 Recd Date 10/11/2002 <br /> Sample Date 10/07/2002 Prep Date 10/13/2002 <br /> Sample Time 1722 Analysis Date 10/13/2002 <br /> Matrix Water QC Batch WMS21748 <br /> Basis Not Filtered Notes <br /> EAnalyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 03 5 PQL NO UG/L 1 <br /> Ethyl tert-butyl ether(ETBE) 05 5 PQL NO UG/L 1 <br /> tert-Amyl methyl ether(TAME) 03 5 PQL NO UG/L 1 <br /> Di-isopropyl ether(DIPE) 05 5 PQL ND UG/L 1 <br /> E tert-Butyl alcohol (TBA) 46 10 PQL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-Bromofluorobenzene 65-135 SMEA 964% 1 <br /> E Toluene-d8 77-150 SMEA 1106% 1 <br /> Dibromofluoromethane 57-156 SMEA 1014% 1 <br /> E <br /> E <br /> E <br /> E <br /> E <br /> E <br /> E <br /> • <br /> E <br /> Approved by l Date 4A L21 <br /> E <br />