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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9470-1 <br /> Lab Control Spike/ Method: 8270C <br /> Lab Control Spike Duplicate Recovery Report- Batch: 720-22674 Preparation: 3550B <br /> LCS Lab Sample ID:LCS 720-22674/2-AA Analysis Batch: 720-22732 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22674 Lab File ID: c:\saturnws\epdata\data\20 <br /> Dilution: 1.0 Units: ug/Kg Initial Weight/Volume: 30.26 g <br /> Date Analyzed: 06/14/2007 1808 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/14/2007 0627 Injection Volume: <br /> LCSD Lab Sample ID:LCSD 720-22674/3-AA Analysis Batch: 720-22732 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22674 Lab File ID: c:\saturnws\epdata\data\200 <br /> Dilution: 1.0 Units: ug/Kg Initial Weight/Volume: 30.12 g <br /> Date Analyzed: 06/14/2007 1837 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/14/2007 0627 Injection Volume: <br /> % Rec. <br /> Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual <br /> Naphthalene 67 60 21 - 133 10 35 <br /> Acenaphthene 62 60 40- 145 3 35 <br /> Acenaphthylene 54 59 33- 145 9 35 <br /> Fluorene 69 66 50- 121 3 35 <br /> Phenanthrene 68 64 10- 130 6 35 <br /> Anthracene 71 67 27- 133 4 35 <br /> Benzo[a]anthracene 68 66 33- 143 3 35 <br /> Chrysene 75 72 17- 168 4 35 <br /> Benzo[a]pyrene 76 74 17- 163 2 35 <br /> Benzo[b]fluoranthene 76 79 24- 159 5 35 <br /> Benzo[k]fluoranthene 79 75 11 - 162 5 35 <br /> Benzo[g,h,i]perylene 76 76 9-219 0 35 <br /> Indeno[1,2,3-cd]pyrene 75 76 9- 171 2 35 <br /> Fluoranthene 71 68 26- 137 3 35 <br /> Pyrene 74 70 52- 115 5 35 <br /> Dibenz(a,h)anthracene 78 81 9- 171 4 35 <br /> Surrogate LCS% Rec LCSD % Rec Acceptance Limits <br /> 2-Fluorobiphenyl 64 61 30- 115 <br /> Terphenyl-d14 80 74 18- 137 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 49 of 55 06/19/2007 <br />