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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9470-1 <br /> Matrix Spike/ Method: 8270C <br /> Matrix Spike Duplicate Recovery Report- Batch: 720-22674 Preparation: 3550B <br /> MS Lab Sample ID: 720-9470-1 Analysis Batch: 720-22732 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22674 Lab File ID: c:\saturnws\epdata\data\2 <br /> Dilution: 1.0 Initial Weight/Volume: 30.37 g <br /> Date Analyzed: 06/14/2007 2032 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/14/2007 0627 Injection Volume: <br /> MSD Lab Sample ID: 720-9470-1 Analysis Batch: 720-22732 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22674 Lab File ID: c:\saturnws\epdata\data\20 <br /> Dilution: 1.0 Initial Weight/Volume: 30.22 g <br /> Date Analyzed: 06/14/2007 2101 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/14/2007 0627 Injection Volume: <br /> % Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Naphthalene 59 62 21 - 133 5 35 <br /> Acenaphthene 54 61 40- 145 13 35 <br /> Acenaphthylene 54 54 33- 145 0 35 <br /> Fluorene 61 68 50- 121 11 35 <br /> Phenanthrene 60 69 10- 130 15 35 <br /> Anthracene 63 72 27- 133 15 35 <br /> Benzo[a]anthracene 57 64 33- 143 12 35 <br /> Chrysene 64 74 17- 168 15 35 <br /> Benzo[a]pyrene 64 77 17- 163 18 35 <br /> Benzo[b]fluoranthene 66 79 24- 159 18 35 <br /> Benzo[k]fluoranthene 67 81 11 - 162 19 35 <br /> Benzo[g,h,i]perylene 66 82 9-219 22 35 <br /> Indeno[1,2,3-cd]pyrene 64 76 9- 171 19 35 <br /> Fluoranthene 63 74 26- 137 16 35 <br /> Pyrene 61 68 52- 115 12 35 <br /> Dibenz(a,h)anthracene 67 82 52- 115 20 35 <br /> Surrogate MS% Rec MSD % Rec Acceptance Limits <br /> 2-Fluorobiphenyl 57 63 30- 115 <br /> Terphenyl-d14 64 75 18- 137 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 50 of 55 06/19/2007 <br />