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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9471-1 <br /> Lab Control Spike/ Method: 8270C <br /> Lab Control Spike Duplicate Recovery Report- Batch: 720-22686 Preparation: 3550B <br /> LCS Lab Sample ID:LCS 720-22686/2-AA Analysis Batch: 720-22826 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22686 Lab File ID: c:\saturnws\epdata\data\20 <br /> Dilution: 1.0 Units: ug/Kg Initial Weight/Volume: 30.37 g <br /> Date Analyzed: 06/15/2007 1828 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/14/2007 1147 Injection Volume: <br /> LCSD Lab Sample ID:LCSD 720-22686/3-AA Analysis Batch: 720-22826 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22686 Lab File ID: c:\saturnws\epdata\data\200 <br /> Dilution: 1.0 Units: ug/Kg Initial Weight/Volume: 30.34 g <br /> Date Analyzed: 06/15/2007 1857 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/14/2007 1147 Injection Volume: <br /> % Rec. <br /> Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual <br /> Naphthalene 65 60 21 - 133 8 35 <br /> Acenaphthene 62 60 40- 145 3 35 <br /> Acenaphthylene 67 62 33- 145 8 35 <br /> Fluorene 71 67 50- 121 6 35 <br /> Phenanthrene 70 64 10- 130 10 35 <br /> Anthracene 69 64 27- 133 8 35 <br /> Benzo[a]anthracene 74 74 33- 143 0 35 <br /> Chrysene 78 75 17- 168 4 35 <br /> Benzo[a]pyrene 68 67 17- 163 2 35 <br /> Benzo[b]fluoranthene 76 73 24- 159 3 35 <br /> Benzo[k]fluoranthene 73 74 11 - 162 1 35 <br /> Benzo[g,h,i]perylene 73 71 9-219 3 35 <br /> Indeno[1,2,3-cd]pyrene 77 73 9- 171 5 35 <br /> Fluoranthene 73 68 26- 137 8 35 <br /> Pyrene 73 72 52- 115 2 35 <br /> Dibenz(a,h)anthracene 77 80 9- 171 4 35 <br /> Surrogate LCS% Rec LCSD % Rec Acceptance Limits <br /> 2-Fluorobiphenyl 71 65 30- 115 <br /> Terphenyl-d14 78 74 18- 137 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 50 of 56 06/19/2007 <br />