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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9471-1 <br /> Matrix Spike/ Method: 8270C <br /> Matrix Spike Duplicate Recovery Report- Batch: 720-22686 Preparation: 3550B <br /> MS Lab Sample ID: 720-9471-19 Analysis Batch: 720-22826 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22686 Lab File ID: c:\saturnws\epdata\data\2 <br /> Dilution: 1.0 Initial Weight/Volume: 30.14 g <br /> Date Analyzed: 06/15/2007 2024 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/14/2007 1147 Injection Volume: <br /> MSD Lab Sample ID: 720-9471-19 Analysis Batch: 720-22826 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22686 Lab File ID: c:\saturnws\epdata\data\20 <br /> Dilution: 1.0 Initial Weight/Volume: 30.09 g <br /> Date Analyzed: 06/15/2007 2053 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/14/2007 1147 Injection Volume: <br /> % Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Naphthalene 49 52 21 - 133 6 35 <br /> Acenaphthene 50 52 40- 145 4 35 <br /> Acenaphthylene 51 53 33- 145 2 35 <br /> Fluorene 56 57 50- 121 1 35 <br /> Phenanthrene 60 57 10- 130 5 35 <br /> Anthracene 59 55 27- 133 8 35 <br /> Benzo[a]anthracene 70 64 33- 143 9 35 <br /> Chrysene 74 68 17- 168 8 35 <br /> Benzo[a]pyrene 65 61 17- 163 7 35 <br /> Benzo[b]fluoranthene 70 67 24- 159 4 35 <br /> Benzo[k]fluoranthene 70 67 11 - 162 4 35 <br /> Benzo[g,h,i]perylene 67 63 9-219 5 35 <br /> Indeno[1,2,3-cd]pyrene 72 66 9- 171 8 35 <br /> Fluoranthene 67 60 26- 137 10 35 <br /> Pyrene 67 62 52- 115 7 35 <br /> Dibenz(a,h)anthracene 74 68 52- 115 7 35 <br /> Surrogate MS% Rec MSD % Rec Acceptance Limits <br /> 2-Fluorobiphenyl 51 57 30- 115 <br /> Terphenyl-d14 73 66 18- 137 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 51 of 56 06/19/2007 <br />