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110 Second Avenue South,##D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INCTelephone 925-798-1620 Fax 925-798-1622 <br /> _J h9R,(iw1,3w.mccam2hell.com E-mail main@mccampbell com <br /> J <br /> Advanced GeoEnvuonmental Client Project ID M <br /> #0450, BP Date Sampled 08/18/98 <br /> 4005 North Wilson Way Date Received 08/19/98 <br /> ' Stockton, CA 95205 Client Contact Bill Little Date Extracted 08121-08124/98 <br /> ' Client P O Date Analyzed 08121-08/24/98 <br /> Volatile Organics By GCIMS <br /> EPA method 8260 <br /> Lab ID 93684 <br /> Client ID BW1-8118198 <br /> Matrix W <br /> Compound Concentration" Compound Concentration' <br /> Acetone ND<10 Ethyibenzene 530 <br /> Benzene 880 Hexachlorobutadiene ND<5 <br /> Bromobenzene ND<S Iodomethane ND<5 <br /> Bromocbloromethane ND<5 Isopropylbenzene 39 <br /> Bromodichloromethane ND<5 p Isopropyl toluene ND<5 <br /> Bromofonn ND<5 Methyl butyl ketone ND_5 <br /> ' Bromomethane ND<5 Methylene Chloride") ND<5 <br /> n-Butyl benzene 17 Methyl ethyl ketone ND<5 <br /> sec-Butyl benzene 82 Methyl isobutyl ketone ND<5 <br /> tert-Butyl benzene ND<5 Methyl tert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<5 Napthalene ND<20 <br /> Carbon Tetrachloride ND<5 n-Propyl bcnzcne 83 <br /> Chlombenzene ND<5 Styrene MND<5 <br /> Chloroethane ND<5 1,1,1,2-Tetrachloroethane ND<5 <br /> ' 2-Chloroethyl Vinyl Ethe ND<5 1,1,2,2-Tetrachloroethane ND<5 <br /> Chloroform ND<5 Tetrachloroethene ND<6 <br /> Chloromethane ND<5 Toluene 1200 <br /> 2-Chlorotoluene ND<5 1,2,3-Tnchlorobenzene ND<5 <br />' 4-Chlorotoluene NEKS 1,2,4-Tnehlorobenzcne ND<5 <br /> Dibromochloromethane ND<5 1,1,1-Tnchloroethane ND<5 <br /> 1,2-Dibromo-3-chloropropane ND<5 1,1,2-Tnchloroethane ND<5 <br /> Dibromomethane N15<5 Trichloroethene ND<5 <br />' 1,2-Dichlorobenzene ND<5 Trichlorofluoromethane ND<5 <br /> 1,3-Dichlorobenzene I ND<5 1,2,3-Tnchloropropane ND<5 <br /> 1,4-Dichloroben7.ene ND<5 1,2,4-Tnmethylbenzene 630 <br /> Dichlorodifluoromethane ND<5 1,3,5-Trtmethylbenzene 200 <br />' ],l-Dichloroethane ND<5 Vinyl Acetate"I l I <br /> 1,2-Dichloroethane ND<5 Vinyl Chloride ° ND<5 <br /> 1,1-Dichlorocthene ND<5 Xylenes,total 3100 <br /> cis-1,2-Drehloroethene ND<5 <br />' trans-1,2-Dichloroethene ND<5 <br /> 1,2-Dichloropropane ND<5 <br /> 1,3-Dichloropropane ND<5 <br /> 2,2-Dichioropmpane ND<5 Comments J <br /> T 1,1-Dichloropropene ND<5 Surrogate Recoveries <br /> cis-1,3-13ichloropropene - NDS Dibromolluoromethane -106 <br /> trans-],3-Drchloropropene ND<5 Toluene-d8 94 <br /> Ethylene drbromide ND<5 4-Bmmolluorobenzene 97 <br />' 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes m ugtmpe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/1.,, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or drrriethyl ketone, (c) (2-chlonoethoxy) ethene, (d)2-hexanone, (e) dichloromethane, (f)2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone,(h)lighter than water irnmiscible sheen is present,(1)liquid sample that contains greater than --5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,0)methylbenzene,(m)acenc acid ethenyl ester,(n)chloroethane,(o)dimethylbenzenes <br />' DHS Certification No 1644 Edward Hanulton,Lab Director <br />