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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> ' MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 halyvlwir.mgcamnbell.com E-mail main@mccampbell com <br /> n <br /> Advanced GeoEnvironmental Client Project ID #0450,MBP Date Sampled 08/18/98 <br /> 4005 North Wilson Way Date Received 08/19/98 <br /> Stockton,CA 95205 Client Contact Bill Little Date Extracted 08121-08124/98 <br /> ' Client P O Date Analyzed 08121-08/24/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> ' Lab ID 93685 <br /> Client ID BW2-8/18/98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<2 Ethylbenzene 46 <br /> Benzene 18 Hexachlorobutadiene ND<2 <br /> Bromobenzene ND<2 Iodomethane ND<2 <br /> Bromochloromethane ND<2 lsopropylbenzene 46 <br /> Bromodichloromethane ND<2 p-Isopropyl toluene ND<2 <br /> Womoform ND<2 Methyl butyl ketone ND<2 <br /> ' Bromomethane ND<2 Methylene Chloride` ND<2 <br /> n-Butyl benzene 28 Methyl ethyl ketone ND<2 <br /> sec-Butyl benzene 3 8 Metbyl isobutyl ketone ND<2 <br /> tent-Butyl benzene ND<2 Methyl tert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<2 Napthalene ND<3 <br /> Carbon Tetrachlonde ND<2 n-Propyl benzene 1 g <br /> Chlorobenzene ND<2 Styrene ND<2 <br /> Chloroethane ND<2 1,1,1,2-Tetrachloroethane ND<2 <br />' 2-Chloroethyl Vinyl Ether` ND<2 1,42,2-Tetrachloroethane ND<2 <br /> Chloroform ND<2 Tetrachloroethene 23 <br /> Chloromethane ND<2 Toluene ND<2 <br /> 2-Chlorotoluene ND<2 1,2,3-Tnchlorobenzene ND<2 <br /> 4-Chlorotoluene ND<2 1,2,4-Tnchlorobenzene ND<2 <br /> Dibromochloromethane ND<2 1,1,1-Tnchloroethane ND<2 <br /> 1,2-13ibromo-3-chloropropane ND<2 1,42-Trichloroethane ND<2 <br /> Dibromomethano ND<2 Trichloroethene 65 <br />' 1,2-Dichlorobenzene ND<2 Trichlorofluoromethane ND<2 <br /> 1,3-Dichlorobenzene ND<2 1,2,3-Tnchloropropane ND<2 <br /> 1,4-Dichlorobenzene ND<2 1,2,4-Tnmethylbenzene ND<2 <br /> Dichlorodifluoromethane ND<2 1,3,5-Tnmethylbenzene ND<2 <br />' 1,1-Dichloroethane ND<2 Vinyl Acetate m 1 6 <br /> 1,2-I)ichloroethane 70 Vinyl Chloride ND<2 <br /> 1,1-Dichloroethene ND<2 Xylenes,total 4 9 <br /> cis-1,2-Drchloroethene 3 2 <br />' trans-1,2-Dichloroethene ND<2 <br /> 1,2-Dichloropropane ND<2 <br /> 1,3-Dichioropropane ND<2 <br /> 2,2-Dichloropropane ND<2 Comments <br />' 1,1-13ichloropropene ND<2 Surrogate Recovenes(%) _ <br /> cis-1,3-Dichloropropene ND<2 Dibromofluoromethane 102 <br /> trans-1,34hchloropropene ND<2 Toluene-d8 97 <br />' Ethylene 1,b mile ND<2 4-Bromofluorobenzene 95 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 10 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> �y 0 2ug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c)(2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone. (g) 4-methyl-2- <br /> pentanone or isopropylacetone,(h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than—5 vol % <br /> sediment,{1}sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,0)methylbenzene,(m)acetic acid ethenyl ester,(n)chlorcethene,(o)dimethylbenzenes <br />' DHS Certification No 1644 ♦ Edward Hanulton,Lab Director <br />