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1 <br /> McCamabell Analytical, Inc. 1534 Willow PassRoad,Pittsburg,CA 94565-1701 <br /> 1 Web:www.mccemp6ell.com E-mail:main@mccamplell.com <br /> "When Oualim Counts" T Telephone:877-252-9262 Fax:925-252-9269 <br /> QC SUMMARY REPORT FOR SM3500 Fe B4c <br /> 1 W.O.Sample Matrix: Water QC Matrix: Water BatchlD: 44744 WorkOrder 0907603 <br /> EPA Method SM3500-Fe B4c Extraction SM3500-Fe 134c Spiked Sample ID: 0907603-007F <br /> ' Sample Spiked MS MSD MS-MSO LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> Analyte <br /> pg/L pg/L %Rec. %Rec. %RPD %Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> Ferrous Iron 1200 200 118 110 1.16 99 104 5.26 70- 130 20 80- 120 1 20 <br /> All target compounds in the Method Blank of this extraction batch were NO less than the method RL with the following exceptions: <br /> NONE <br /> 1 BATCH 44744 SUMMARY <br /> 1 Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0907603-OOIF 07/22/09 2:20 PM 07/23/09 07/23/094:01 PM 0907603-002F 07/22/09 1:25 PM 07/23/09 07/23/09 4:07 PM <br /> 0907603-003F 07/22/09 12:10 PM 07/23/09 07/23/09 4:13 PM 0907603-004F 07/22/09 10:20 AM 07/23/09 07/23/09 4:19 PM <br /> 0907603-OOSF 07/22/09 4:00 PM 07/23/09 07/23/09 4:25 PM <br /> 1 <br /> 1 <br /> 1 <br /> t <br /> 1 <br /> 1 <br /> 1 <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)12', <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons'.a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> ' WA=not applicable to this method. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification 1644 QA/QC Officer <br />