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534 <br /> Q McCamabell Analytical. Inc. :www.mllow Pass Road,Pittsburg,-mail: ain 94565-1701 <br /> Web:www.mcwmpbell.com E-mail:meinQmwampbell.com <br /> "When Oualily Counts" T Telephone,877-252-9262 Fax:925-252-9269 <br /> QC SUMMARY REPORT FOR SM5210B <br /> W.O.Sample Matrix: Water OC Matrix: Water BatchlD: 44673 WorkOrder 0907603 <br /> EPA Method SM5210B Extraction SM6210B Spiked Sample ID: NIA <br /> ' <br /> Analyte Sample Spiked I MS I MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/L mg/L I%Rec. %Rec. %RPD I%Rec. %Rec. %RPD I MS/MSD I RPD LCS/LCSD RPD <br /> BOD N/A 198 1 N/A N/A N/A 1 98.7 1 98.7 0 1 N/A I N/A 80- 120 1 16 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> ' BATCH 44673 SUMMARY <br /> ' Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0907603-001 B 07/22/09 2:20 PM 07/22/09 07/28/09 3:20P <br /> 0907603-002B 07/22/09 1:25 PM 07/22/09 07/28/09 3:26 PM <br /> 0907603-0038 07/22/09 12:10 PM 07/22/09 07/28/09 3:38 PM 0907603-004B 07/22/09 10:20 AM 07/22/09 07/28/09 3:50 PM <br /> 0907603-005B 07/22/09 4:00 PM 07/22/09 07/28/09 4:08 PM <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> ' %Recovery=100'(MS-Sample)I(Amount Spiked);RPD=100'(MS- MSD)I((MS+MSD)12). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following mason&,a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> ' N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted dueto high matrix or analyte <br /> uel. content <br /> ' DHS ELAP Certification 1644 QA/QC Officer <br />