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Date Wo,k O,der <br /> 09āœ“uā€ž-oo Alpha Analytical, Inc - C Summary Report <br /> 00060240 <br /> Method Blank Test Code SW8015 Batch ID MS6S0605B Analysis Date 06/06/2000 00 58 <br /> Sample ID MBLK MS6S060SAIS Units mg1Kg Run ID GCIMSD_6_000605 Prep Date 06/06/2000 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> PH Purgeable ND 1 <br /> Surr 1,2-Dichloroethane-d4 0 189 02 95 68 139 <br /> Surr Toluene-d8 0204 D 2 102 75 127 <br /> Surr 4-Bromofluorobenzene 0 19 0 2 95 73 128 <br /> Laboratory Control Spike Test Code SW8015 Batch 0 MS6S0605B Analysis Date 06/05/2000 23 41 <br /> Sample ID GLCS M56SO605B Units mglKg Run lD GCIMSD_6_000605 Prep Date 06105/2000 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Hightimit RPD Ref Val %RPD Qual <br /> TPH Purgeable 9 37 1 8 117 43 141 <br /> Surr 1,2-Dichloroethane-d4 0 219 0 2 110 68 139 <br /> Surr Toluene-d8 0 195 0 2 97 75 127 <br /> Surr 4-Bromofluorobenzene 0 188 0 2 94 73 128 <br /> Sample Matrix Spike Test Code SW8015 Batch ID MS6S0605B Analysis Date 06106/2000 08 36 <br /> Sample ID 00060243-02AGS Units mg/Kg Run ID GCIMSD_6_000605 Prep Date 06/0612000 <br /> Analyte Result PQL SpkVal SpkRefVal %PEC LowLimit 4ghl-emit RPD Ref Val %RPD Qual <br /> TPH Purgeable 47 5 5 40 0 119 43 141 <br /> Surr 1 2-Dichloroethano-d4 1 03 1 103 68 139 <br /> Surr Toluene-d8 1 03 1 103 75 127 <br /> Surr 4-Bromofluorobenzene 1 04 1 104 73 128 <br /> Sample Matrix Spike Duplicate Test Code SW8015 Batch 11) MS6S0605B Analysis Date 06/06/2000 09 02 <br /> Sample ID 00060243-02AGSD Units mg/Kg Run ID GC/MSD-6-000605 Prep Date 06/06/2000 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit High Limit RPD Ref Val %RPD Qual <br /> TPH Purgeable 46 3 5 40 0 116 43 141 47 53 266 <br /> Surr 1 2-Dichloroethane-d4 1 04 1 104 68 139 <br /> Surr Toluene-d8 1 02 1 102 75 127 <br /> Surr 4-Bromofluorobenzene 0 995 1 99 73 128 <br /> I <br /> Comments ND-Not Detected at the Reporting Limit D-if the spiked value,s<25%of the reference value,recovery should not be calculated <br /> S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery hmits due to matrix <br /> 2-Analyte detected in the associated Method Blank <br />