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1).;, Work Order <br /> ov-ru,-aa Alpha Analytical, Inc - QC Sun=arY Report <br /> 00060240 <br /> Method Blank Test Code SW8260B Batch lD MS6S0605A Analysis Date 0610612000 00 58 <br /> Sample 0 MBLK MS6S0605A/B Units pg/Kg Run lD GC/MSD_6_000605 Prep Date 06/06/2000 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit High Limit RPD Ref Val %RPD Qual <br /> Tertiary Butyl Alcohol(TBA) ND 500 <br /> Methyl tert-butyl ether(MTBE) ND 5 <br /> Di-isopropyl Ether(DIPE) ND 20 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 20 <br /> 12-Dichloroethane ND 20 <br /> Benzene ND 5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 20 <br /> Toluene ND 5 <br /> 12-Dibromoethane ND 40 <br /> Ethylbenzene ND 5 <br /> m,p-Xylene ND 5 <br /> o-Xylene ND 5 <br /> Surr 1,2-Dichloroethane-d4 189 200 95 70 131 <br /> Surr Toluene-d8 204 200 102 74 138 <br /> Surr 4-Bromofluorobenzene 190 200 95 59 133 <br /> Laboratory Control Spike Test Code SW8260B Batch ID MS6S0605A Analysis Date 06/05/2000 22 50 <br /> Sample ID LCS MS6S0605A Units pg/Kg Run ID GCIMSD_6-000605 Prep Date 06/05/2000 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HsghLimct RPD Ref Val %RPD Qual <br /> Methyl tent-butyl ether(MTBE) 187 5 200 93 70 142 <br /> Benzene 180 5 200 90 fib 142 <br /> Toluene 203 5 200 102 59 139 <br /> Ethylbenzene 212 5 200 106 70 134 <br /> m p-Xylene 472 5 400 118 60 146 <br /> o-Xylene 236 5 200 118 52 148 <br /> Surr 1 2-Dichloroeth2ne-d4 209 200 104 70 131 <br /> Surr Toluene-d8 197 200 98 74 138 <br /> Surr 4-Bromofluorobenzene 215 200 107 59 133 <br /> Sample Matrix Spike Test Code SW8260B Batch ID MS6So605A Analysis Date 06/06/2000 09 27 <br /> Sample 0 00060243-02AMS Units pg/Kg Run ID GCIMSD_6_000605 Prep Date 06106/2000 <br /> nalyte Result PQL SpkVal SpkRefVal %REC LowLimit Hight-imit RPD Ref Val %RPD Qual <br /> Methyl tent-butyl ether(MTBE) 905 25 1000 0 91 70 142 <br /> Benzene 954 25 1000 0 95 66 142 <br /> Toluene 1040 25 1000 0 104 59 139 <br /> Ethylbenzene 1090 25 1000 0 109 70 134 <br /> m p-Xylene 2300 25 2000 0 115 60 146 <br /> o-Xylene 1180 25 1000 0 118 52 148 <br /> Surr 1,2-Dichloroeth2ne-d4 1030 1000 103 70 131 <br /> Surr Toluene-d8 1010 1000 101 74 138 <br /> Surr 4-Bromofluorobenzene 1100 1000 110 59 133 <br /> Sample Matrix Spike Duplicate Test Cade SW8260B Batch ID MS6S0605A Analysis Date 06/06/2000 09 52 <br /> Sample ID 00060243-02AMSD Units pg1Kg Run ID GCIMSD_6_000605 Prep Date 06/0612000 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> Methyl tert-butyl ether(MTBE) 828 25 1000 0 83 70 142 9053 8 97 <br /> Benzene 912 25 1000 0 91 66 142 9543 4 58 <br /> Toluene 1040 25 1000 0 104 59 139 1039 0 312 <br /> Ethylbenzene 1110 25 1000 0 ill 70 134 1088 244 <br /> m,p-Xylene 2360 25 2000 0 118 60 146 2297 2 67 <br /> o-Xylene 1170 25 1000 0 117 52 148 1179 0 506 <br /> Surr 1 2-Dichloroeth2ne-d4 980 1000 98 70 131 <br /> Surr Toluene-d8 1050 1000 105 74 138 <br /> Surr 4-Bromofluorobenzene 1160 1000 116 59 133 <br /> Comments ND-Noi Detected at the Reporting Limit D-if the spiked value is Q.)%of the iefeience�alue recovei y should not be calculated <br /> 5-Spike Recovery outside accepted iecoveiy limits M-4pike Recoveiy outside accepted recovery limits due to matrix <br /> B Analyte detected to the associated Method Blank <br />