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N <br /> + r <br /> Date <br /> 2;-Aug-01 Alpha Analytical, Inc - QC Summary Report Fork Order <br /> 01082062 <br /> Method $lank Type MBLK Test Code SW8015 Batch ID MS9W0821D <br /> File ID D tHPCHEMlMS081DATA1010821101082137 D Analysis Date 08/22/2001 02 15 <br /> Sample ID MBLK MSBW0821 B Units mglL Run ID GC/MSD_B_010821 B Prep Date 0812212001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable ND 005 <br /> Surr 1 2-Dichloroethane-d4 000985 0 01 98 71 130 <br /> Surr Toluene-d8 000961 0 01 96 69 127 <br /> Surr 4-Bromofluorobenzene 00104 001 104 80 123 <br /> Laboratory Control Spike Type LCS Test Code SW8015 Batch 0 MS9W0821D <br /> File ID D 1HPCHEM\M5081DATA1010821101062136 D Analysts Date 08/22/2001 01 49 <br /> Sample ID GLCS MS8W0821D Units mglL Run ID GCIMSD_8_010821B Prep Date 08/22/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLtmit RPD Ref Val %RPD Qua[ <br /> TPH Purgeable 0 414 005 0 4 103 58 136 <br /> Surr 1 2-DicNoroethane-d4 00102 0 01 102 71 130 <br /> Surr Toluene-d8 000828 0 01 83 69 127 <br /> Surr 4-Bromofluorobenzene 000971 0 01 97 BO 123 <br /> Sample Matrix Spike Type MS Test Code SW8015 Batch ID MS9W0821 D <br /> File ID D IHPCHEM1MS081DATA1010821101082158 D Analysis Date 08/22/2001 11 20 <br /> Sample ID 01082062-OIAGS Units mg1L Run ID GCIMSD_8_0108218 Prep Date 08!2212001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LOWLimit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable 1 65 025 2 00523 80 58 136 <br /> Surr 1 2-Dichloroethane-d4 00521 005 104 71 130 <br /> Surr Toluene-d8 00445 005 89 69 127 <br /> Surr 4-Bromofluorobenzene 00457 005 91 80 123 <br /> Sample Matrix Spike Duplicate 4 Type MSD Test Code SW8015 Batch ID MS9W0821D <br /> File ID D1HPCHEMLMS08�DATA1010821101082159 D Analysis Date 06/2212001 11 46 <br /> Sample ID 01082062-01AGSD Units mglL Run ID GC/MSD_B_010821B Prep Date 08/22/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br />. TPH Purgeable 1 66 025 2 00523 80 58 136 1 646 0 582 <br /> Surr 1,2-Dichloroethane-d4 00494 005 99 71 130 <br /> Surr Toluene-d8 00447 005 89 65 127 <br /> Surr 4-Bromofluorobenzene 00468 005 94 80 123 <br /> Comments ND Not Detected at the Reporting Limit D-If the spiked value is X25%of the reference value,recovery should not be calculated <br /> S Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix <br /> B-Analyte detected in the associated Method Blank <br />