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G 2?-Aug-or Alpha Analytical, Inc _ QC Summary Report Work Order 01082062 Method $lank Type MBLK Test Code SW8260B Batch ID MS8W0821C File ID D 1HPCHEM1MS08kDATA1010821101082137 D Analysis Date 08/2212001 02 15 Sample ID MBLK MS8W0821B Units pg1L Run ID GCIMSD_8_010821B Prep Date 0812212001 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual Tertiary Butyl Alcohol(TBA) ND 5 Methyl tert-butyl ether(MTBE) ND 05 a-isopropYl Ether(RIPE) ND 1 Ethyl Tertiary Butyl Ether(ETRE) ND 1 Benzene ND 0 5 Ternary Amyl Methyl Ether(TAME) ND 1 Toluene ND 0 5 Ethylbenzene ND 0 5 m p-Xylene ND 0 5 o-Xylene ND 0 5 Surr 1 2-Dichloroethane-d4 985 10 99 71 130 Surr Toluene-d8 961 10 96 69 127 Surr 4-Bromofluorobenzene 104 10 104 80 123 Laboratol y Control Spike Type LCS Test Code SW82608 Batch ID MSBW0821C File ID D IHPCHEM1MS081DATA1010821k010B2134 D Analysis Date 08/22/2001 00 57 Sample ID LCS MS8W6821C Units pg1L Run ID GCIMSD_8_010821B Prep Date 013/22120011 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual Benzene 11 2 0 5 10 112 80 120 Toluene 104 0 5 10 104 80 120 Ethytbenzene 10 9 0 5 10 109 80 120 m p Xylene 21 6 0 5 20 108 73 129 o-Xylene 107 0 5 10 107 73 127 Surr 1 2-Dichloroethane-d4 10 7 10 107 71 130 Surr Toluene-d8 929 10 93 69 127 Surr 4-Bromofluorobenzene 942 10 94 80 123 Sample Matrix Spike Type NIS Test Code SW8260B Batch ID MS8W0821C File ID D 1HPCHEMIMSDBIDATAk010821101062156 D Analysts Date 08122/2001 10 28 Sample 1D 01082062-01AMS Units pg/L Run ID GC/MS0_8_010821B Prep Date 0812212001 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Quat Benzene 51 5 2 5 50 0 103 80 120 Toluene 47 4 2 5 50 0 95 80 120 Ethylbenzene 49 7 2 5 50 0 99 80 120 m p-Xylene 98 7 2 5 100 0 99 73 129 o-Xylene 48 7 2 5 50 0 97 73 127 Surr 1 2-Dichloroethane-d4 551 50 110 71 130 Surr 7oluene-d8 456 50 91 69 127 Surr 4-Bromofluorobenzene 457 50 91 80 123 Sample Matrix Spike Duplicate Type MSD Test Code SW8260B Batch ID MS8W0821C File ID D1HPCHEMIMS08kDATAk010821101082157 D Analysis Date 08/22/2001 10 54 ' Sample ID 01082062-01AMSD Units pg/L Run ID GCIMSD_6_010821B Prep Date 08/22/2001 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imrt HighLimit RPD Ref Val %RPD Quai Benzene 48 3 2 5 50 0 97 80 120 51 47 638 Toluene 45 2 5 50 0 90 80 120 47 37 518 Ethylbenzene 46 4 2 5 50 0 93 80 120 4973 701 m p Xylene 91 5 25 100 0 91 73 129 98 66 7 57 o-Xylene 462 2 5 50 0 92 73 127 48 69 5 31 Surr 1 2-Dichloroethane-d4 537 50 107 71 130 Surr Toluene-d8 465 50 93 69 127 Surr 4-Bromofluorobenzene 46 4 50 93 80 123 Comments ND-Not Detected at the Reporting Limit D-If the spiked value is X25%of the reference value,recovery should not oe calculated S Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix B Analyte detected in the associated Method Blank