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L0 110 2nd Avenue Sou ,#D7,Pacheco,CA 94553-5560 <br /> MCCAWBELL ANALYTICAL INC. Telephone-925-798-1620 Fax:925-798.1622 <br /> hn://www.mampbell.com mpbell.com E-mail:mainQa mccampbell-com <br /> L <br /> Advanced GeoEnvirotunental Client Project 1D:Stockton Municipal Date Sampled:03/17/00 <br /> 4005 North Wilson Way Service Center Date Received:03/18/00 <br /> LStockton,CA 95205 Client Contact:Bob Marty Date Extracted:03/18/00 <br /> Client P.O: Date Analyzed:03/21-03/23/00 <br /> LVolatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 33410 <br /> L Client ID B1-25' <br /> Matrix S <br /> and Concentration* Compound Concentration" <br /> L Acetone NDXIO trans-1,3-Diehloropropene ND <br /> Beame ND Ethylene dibromide ND <br /> BroRqbenzene ND Ethylbenzene ND <br /> Bromoahloromethane ND Nexachlorobutadiene ND <br /> L Bromodichloromethane ND lodomethane ND <br /> BTorto orm ND Isopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone ND <br /> L sec-Butyl benzene ND Methylene Chloride ND <br /> ten-Butyl benzene ND Methyl ethyl ketone ND <br /> Carbon Disulfide ND Methyl isobutyl ketone w ND <br /> Carbon Tetrachloride ND Methyl ten-Butyl Ether(MTBE) — <br /> L Chlorobenzene ND Naphthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether") ND Styrene ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> L Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene ND <br /> L Dibromochloromethane ND 1,2,3-Trichlorobenzene ND <br /> 1,2-Dibromo-3-chloropropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND 10,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br /> L 1,3-Dichlorobenzenc ND Trichloroethene ND <br /> 1,4-Dichlorobenzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND <br /> 1,1-Droe <br /> ichlothane ND 1,2,4-Trimethylbenzene ND <br /> L 1,2-Dichloroethane ND 1,3,5-Trimethylbenzene ND <br /> 1,1-Dichloroethene ND Vinyl Acetate ND <br /> cis-1,2-Dichlotoethene ND Vinyl Chloride ND <br /> trans-1 - ichloroet ene ND Xylenes,total ND <br /> L 1,2-Dichloropropane ND Comments: <br /> 1,3-Dichlompropane ND Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND Dibromofluoromethane 90 <br /> 1,1-Dichloropropene ND Toluene-d8 107 <br /> k cis-1,3-Dichloropropene 4-Bromo uombenzene 1 108 <br /> L 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ]reporting limits unless otherwise stated:water samples l ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit:N/A means analyte not applicable to this analysis <br /> (b)2-propanone or dimethyl ketone; (c)(2-chloroethoxy)ethene;(d)2-hexanone•,(e)dichloromethane;(1)2-butanone; (g)4-methyl-2- <br /> pentanone or isopropylacetone;(h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than–5 vol.% <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> L <br />