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L110 Id Avenue Sou ,#D7,Pacheco,CA 94553-5560 <br /> MCCAWBELL ANALYTICAL INC. Telephone:925.798-1620 Fax:925-798-1622 <br /> Lhttp://www.mccan7pbell.com E-mail:main@mccampbell.com <br /> LAdvanced GeoEnvironmental Client Project ID:Stockton Municipal Date Sampled:03/17/00 <br /> 4005 North Wilson Way Service Center Date Received:03/18/00 <br /> LStockton,CA 95205 Client Contact:Bob Marty Date Extracted:03/18/00 <br /> Client P.O: Date Analyzed:03/21-03/23/00 <br /> LVolatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 33416 <br /> L Client ID 132-25' <br /> Matrix S <br /> C2=d Concentration* Compound Concentration* <br /> L Acetone ND<10 trans-1,34)ichloropropene ND <br /> Benzene ND &hylene dibromide ND <br /> Bromobenzene ND Ethylbenzene _N D <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> L Bromodichloromethane ND lodomethane ND <br /> Bromoform ND Isopropylbenzene ND <br /> Bromometbane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone ND <br /> L sec-Butyl benzene ND Methylene Chloride ND <br /> tert-Butyl benzene ND Methyl ethyl ketone ND <br /> Carbon Disuifide ND Methyl isobutyl ketone 00 ND <br /> Carbon Tetrachloride ND Methyl tent-Butyl Ether(MTBE) --- <br /> L Chlorobenzene ND Naphthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether') ND Styrene W ND <br /> Chloroform ND 10,1,2-Tetrach1oroethane ND <br /> L Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlarotoluene ND Toluene ND <br /> Dibromochloromethane ND 1,2,3-Trichlorobenzene ND <br /> L 1,2-Dibromo-3-chloropropane ND 1,2,4- richlorobenzene ND <br /> Dibromomethane ND 1,1,1-Tricbloroethane ND <br /> 1,2-1:)ichlorobenzene ND 1,1,2-Trichloroethane ND <br /> l,3-Dichlorobenzene ND Trichloroethene ND <br /> L 1,4-Dichlorobenzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND <br /> 1,1-Dichloroethane ND 1,2,4-Trimethylbenzene ND <br /> L 1,2-1)ichloroethane ND 1,3,5-Trimethylbenzene ND <br /> 1,1-DichloroetIme ND Vinyl Acetate ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride ND <br /> trans-l,2-Dichlomethene ND Xylenes,total ND <br /> L <br /> 1 <br /> ,2-Dichloropropane ND Comments: <br /> 1,3-Dichloropropane ND Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND Dibromofluoromethane 99 <br /> 1,1-Dichloropropene ND Toluene-d8 97 <br /> L cis-1, - ichloropropene ND 4-Bromofluorobenzene 104 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> L ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b)2-propanone or dimethyl ketone;(c)(2-chloroethoxy)ethene; (d)2-hexanone;(e)dichloromethane; (f)2-butanone•, (g)4-methyl-2- <br /> pentanone or isopropylacetone;(h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than--5 vol.% <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene, (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> L chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br /> L <br />