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September 7, 2006 Lab ID STK636936 <br /> Alpine Packing Company Customer 3002839 <br /> Quality Control: <br /> Inorganic - Metals QC <br /> 200.7 08/16/2006:13203 Continued... <br /> on the LCS or CCV recovery. <br /> 08/17/2006:A IT203 All analysis quality controls are within established criteria. <br /> Inorganic - Wet Chemistry QC <br /> 2510B 08/15/2006:A212 All preparation quality controls are within established criteria. <br /> O8/15/2006:A - EC201 All analysis quality controls are within established criteria. <br /> 2540C 08/15/2006:A235 All preparation quality controls are within established criteria. <br /> 300.0 08/14/2006:A215 All preparation quality controls are within established criteria, except: <br /> The following note applies to Chloride: <br /> 435 Sample matrix may be affecting this analyte. Data was accepted based on the <br /> LCS or CCV recovery. <br /> 08/14/2006:A - IC204 All analysis quality controls are within established criteria. <br /> 351.1 08/18/2006:13242 All preparation quality controls are within established criteria, except: <br /> The following note applies to Kjeldahl Nitrogen: <br /> 435 Sample matrix may be affecting this analyte. Data was accepted based on the <br /> LCS or CCV recovery. <br /> 08/22/2006:A242 All preparation quality controls are within established criteria, except: <br /> The following note applies to Kjeldahl Nitrogen: <br /> 408 Matrix Spike(MS) or Post Digestion Spike(PDS) has no Acceptance Range <br /> (DQO) because of high analyte concentration in the sample. Data was accepted based <br /> on the LCS or CCV recovery. <br /> 08/23/2006:13 - FI203 All analysis quality controls are within established criteria. <br /> 08/31/2006:A - F1203 All analysis quality controls are within established criteria. <br /> 4500-H B 08/11/2006:5346 All preparation quality controls are within established criteria. <br /> 08/11/2006:S - PH301 All analysis quality controls are within established criteria. <br /> 4500NO3F 08/18/2006:13220 All preparation quality controls are within established criteria. <br /> O8/22/2006:A220 All preparation quality controls are within established criteria. <br /> 08/21/2006:13 - FI203 All analysis quality controls are within established criteria. <br /> Table continued on next page... <br /> STK636936: Case Narrative Page 2 <br />