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Alpha Analytical, Inc. <br /> l 255 Glendale Ave. • Suite 21 • Sparks,Nevada 8 943 1-5 778 <br /> I� (775)355-1044 • (775)355-0406 FAX• 1-800-283-1183 <br /> ate: ork Order: <br /> ec-OS OC Summary Report W05120803 <br /> Method Blank Type:MBLK Test Code:EPA Method SW8260B <br /> File ID:C:IHPCHEM1MS071DATA1051208105120807.D Batch 1D:MSD7A1208A Analysis Date: 12/08/2005 10:17 <br /> Sample ID: MBLK MS07A1208A Units:mglm3 Run ID:MSD_07_051208B Prep Date: 12/08/2005 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Tertiary Butyl Alcohol(TBA) ND 5 <br /> Methyl tert-butyl ether(MTBE) ND 0.1 <br /> Di-isopropyl Ether(DIPE) ND 0.2 <br /> Ethyl Tertiary Butyl Ether(ETRE) ND 0.2 <br /> Benzene ND 0.1 <br /> Tertiary Amyl Methyl Ether(TAME) ND 0.2 <br /> Toluene ND 0.1 <br /> Ethylbenzene ND 0.1 <br /> m,p-XVlene ND 0.1 <br /> o-XVlene ND 0.1 <br /> Surr; 1,2-Dichloroethane-d4 1.91 2 96 76 127 <br /> Surr.Toluene-d8 1,91 2 96 84 113 <br /> Surr:4-Bromofluorobenzene 1.96 2 98 79 119 <br /> Laboratory Control Spike Type:LCS Test Code:EPA Method SW8260B <br /> File ID:C:IHPCHEMXMS071DATA1051208105120804.D Batch ID:MS07A1208A Analysis Date: 12/08/2005 09:12 <br /> Sample ID: LCS MS07A1208A Units :mglm3 Run ID:MSD_07_051208B Prep Date: 12/08/2005 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Highl-imit RPDRefVal %RPD(Limit) Qual <br /> Benzene 9.25 0.1 10 93 81 122 <br /> Toluene 10.3 0.1 10 103 80 120 <br /> Ethylbenzene 10.2 0.1 10 102 80 120 <br /> m,p-XVlene 10.5 0.1 10 105 80 129 <br /> o-XVlene 10.2 0.1 10 102 80 129 <br /> 1,2-Dichloroethane-d4 9.97 10 99.7 76 127 <br /> Toluene-d8 10.7 10 107 84 113 <br /> r:4-Bromofluorobenzene 9.68 10 97 79 119 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br /> i <br />