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Entech Analytic Labs, Inc. 3334 Victor Court , Santa Clara, CA 95054 Phone: (408) 588-0200 Fax: (408) 588-0201 Compliance&Closure,Inc.-Danville 4115 BlackHawk Plaza Circle Suite 100 Project Number: 12118-2 Danville,CA 94506 Project Name: Quik Stop#121. Attn: Mr.Gary Mulkey GlobalID: T0607700831 Certificate of Analysis - Data Report Samples Received: 09/19/2006 Sample Collected by: Client Lab# : 51433-001 Sample ID: GP-7-10 Matrix: Solid Sample Date: 9/19/2006 9:05 AM VOCs:EPA 8260B Parameter Result Qual D/P-F Detection Limit Units Prep Date Prep Batch Analysis Date QC Batch Benzene ND 1.0 5.0 pg/Kg N/A N/A 9/19/2006 SM3060919 Toluene ND 1.0 5.0 pg/Kg N/A N/A 9/19/2006 SM3060919 Ethyl Benzene ND 1:0 5.0 pg/Kg N/A N/A 9/19/2006 SM3060919 Xylenes,Total ND 1.0 10 pg/Kg N/A N/A 9/19/2006 SM3060919 Methyl-t-butyl Ether ND 1.0 .5.0 pg/Kg N/A N/A 9/19/2006 SM3060919 tert-Butyl Ethyl Ether ND 1.0 5.0 pg/Kg N/A N/A 9/19/2006 SM3060919 tert-Butanol(TBA) ND 1.0 40 pg/Kg N/A N/A 9/19/2006 SM3060919 Diisopropyl Ether ND 1.0 5.0 pg/Kg N/A N/A9/19/2006 SM3060919 tert-Amyl Methyl Ether ND 1.0 5.0 pg/Kg N/A N/A 9/19/2006 SM3060919 Surrogate Surrogate Recovery Control Limits(%) Analyzed by: Mfelix 4-Bromofluorobenzene 83.1 60 130 Reviewed by: MaiChiTu Dibromofluoromethane 88.0 60 130 Toluene-d8 96.6 60 - 130 TPH-Purgeable:GC/MS Parameter Result Qual D/P-F Detection Limit Units Prep Date Prep Batch Analysis Date QC Batch TPH as Gasoline ND 1.0 100 pg/Kg N/A N/A 9/19/2006 SM3060919 Surrogate Surrogate Recovery Control Limits(%) Analyzed by: Mfelix 4-Bromofluorobenzene 85.8 60 130 Reviewed by: MaiChiTu Dibromofluoromethane 94.9 60 130 . Toluene-d8 97.4 60 130 it i Detection Limit=Detection Limit for Reporting. ND=Not Detected at or above the Detection Limit. D/P-F=Dilution and/or Pren Factnr includes samnle volume arlinstments 01=rht.Ili—lir— onnnnnF o cc.in DNA ak.