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Entech Anal tick Labs Inc. ` 3334 Victor Court , Santa Clara, CA 95054 Phone: (408) 588-0200 Fax: (408) 588-0201 Compliance&Closure,Inc.-Danville 4115 B1ackHawk Plaza Circle Suite 100 Project Number: 12118-2 Danville,CA 94506 Project Name:,Quik Stop#121 Attn: Mr.Gary Mulkey GlobalID: T0607700831 Certificate of Analysis - Data Report samples Received: 09/19/2006 Sample Collected by: Client Lab# : 51433-002 Sample ID: GP-7-15 Matrix: Solid SamplelDate: 9/19/2006 9:15 AM VOCs:EPA 8260B Parameter Result Qual D/P-F Detection Limit Units Prep Date Prep Batch Analysis Date QC Batch Benzene ND 1.0 5.0 pg/Kg N/A N/A 9/19/2006 SM3060919 Toluene ND 1.0 5.0 pg/Kg N/A N/A 9/19/2006 SM3060919 Ethyl Benzene ND 1.0 5.0 µg/Kg N/A N/A 9/19/2006 SM3060919 Xylenes,Total ND 1.0 10 pg/Kg N/A N/A 9/19/2006 SM3060919 Methyl-t-butyl Ether ND 1.0 5.0 pg/Kg N/A N/A 9/19/2006 SM3060919 tert-Butyl Ethyl Ether ND 1.0 5.0 pg/Kg N/A N/A� 9/19/2006 SM3060919 tert-Butanol(TBA) ND 1.0 40 pg/Kg N/A" N/A 9/19/2006 SM3060919 Diisopropyl Ether ND 1.0 5.0 pg/Kg N/A N/A 9/19/2006 SM3060919 tert-Amyl Methyl Ether ND 1.0 5.0 pg/Kg N/A N/A 9/19/2006 SM3060919 Surrogate Surrogate Recovery Control Limits(%) Analyzed by: Mfelix 4-Bromofluorobenzene 77.5 60 130 Reviewed by: MaiChiTu Dibromofluoromethane 84.2 60 •- 130 .e Toluene-d8 90.7 60. - . 130 . TPH-Purgeable:GC/MS I Parameter •Result Qual D/P-F. Detection LimitUnits Prep Date Prep Batch Analysis Date QC Batch TPH as Gasoline ND 1.0 100. pg/Kg N/A N/A 9/19/2006 SM3060919 Surrogate Surrogate Recovery Control Limits(%) Analyzed by: Mfelix 4-Bromofluorobenzene 81.8 60 130 Reviewed by: MaiChiTu Dibromofluoromethane 90.5 60 130 Toluene-d8 93.3 60 130 - i I Detection Limit=Detection Limit for Reporting. ND=Not Detected at or,above the Detection Limit. D/P-F=Dilution and/or Prep Factor includes sample volume adjustments. Qual=Data Qualifier 9/20/2006 7:58:10 PM-dba