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Entech Analytic�WLabs, Inc. 3334 Victor Court , Santa Clara, CA 95054 Phone: (408) 588-0200 Fax: (408) 588-0201 Compliance&Closure,Inc.-Danville Project Number: 12118-2 4115 BlackHawk Plaza Circle Suite 100 Project Name: Quik Stop#121 Danville,CA 94506 Attn: Mr.Gary Mulkey GlobalID: T0607700831 Certificate of Analysis - Data Report Samples Received: 09/1.9/2006 Sample Collected by: Client Lab#: 51433-003 Sample ID: GP-8-10 Matrix: Solid Sample Date: 9/19/2006 9:35 AM VOCs:EPA 82608 Parameter Result Qual D/P-F Detection Limit Units Prep Date Prep Batch Analysis Date QC Batch Benzene ND 1.0 5.0 µg/Kg N/A N/A 9/19/2006 SM3060919 Toluene ND 1.0 5.0 gg/Kg N/A N/A 9/19/2006 SM3060919 Ethyl Benzene ND 1.0 5.0 µg/Kg N/A N/A 9/19/2006 SM3060919 Xylenes,Total ND 1.0 10 pg/Kg N/A N/A 9/19/2006 SM3060919 Methyl-t-butyl Ether ND 1.0 5.0 µg/Kg N/A N/A 9/19/2006 SM3060919 tert-Butyl Ethyl Ether ND 1.0 5.0 µg/Kg N/A N/A 9/19/2006 SM3060919 tert-Butanol(TBA) ND 1.0 40 pg/Kg N/A N/A 9/19/2006 SM3060919 Diisopropyl Ether ND 1.0 5.0 gg/Kg N/A N/A 9/19/2006 SM3060919 cert-Amyl Methyl Ether ND 1.0 5.0 µg/Kg N/A N/A 9/19/2006 SM3060919 Surrogate Surrogate Recovery Control Limits(%) Analyzed by: Mfelix 4-Bromofluorobenzene 79.8 60 130 Reviewed by: MaiChiTu Dibromofluoromethane 83.5 60 130 Toluene-d8 92.7 60 130 TPH-Purgeable:GC/MS Parameter Result Qual D/P-F Detection Limit Units Prep Date Prep Batch Analysis Date QC Batch TPH as Gasoline ND 1.0 100 µg/Kg N/A N/A 9/19/2006 SM3060919 Surrogate Surrogate Recovery Control Limits(%) Analyzed by: Mfelix 4-Bromofluorobenzene 84.0 60 130 Reviewed by: MaiChiTu i Dibromofluoromethane 89.4 60 130 Toluene-d8 95.0 60 - 130 I I j i Detection Limit=Detection Limit for Reporting. ND=Not Detected at or above the Detection Limit. D/P-F=Dilution and/or Prep Factor includes sample volume adjustments. Qual=Data Qualifier 9/20/2006 7:58:10 PM-dba I