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Quality Control Results <br /> Client: SECOR International, Inc. Job Number: 720-7408-1 <br /> Method Blank - Batch: 720-17537 Method: 8015B <br /> Preparation: 3550B <br /> Lab Sample ID: MB 720-17537/1-AA Analysis Batch: 720-17745 Instrument ID: HP DRO5 <br /> Client Matrix: Solid Prep Batch: 720-17537 Lab File ID: N/A <br /> Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 30.27 g <br /> Date Analyzed: 01/24/2007 2224 Final Weight/Volume: 5 mL <br /> Date Prepared: 01/24/2007 1348 Injection Volume: <br /> Column ID: PRIMARY <br /> Analyte Result Qual RL <br /> Diesel Range Organics[C9-C24] 1.3 0.99 <br /> Surrogate % Rec Acceptance Limits <br /> o-Terphenyl 80 50-130 <br /> Lab Control Spike/ Method: 8015B <br /> Lab Control Spike Duplicate Recovery Report- Batch: 720-17537 Preparation: 3550B <br /> LCS Lab Sample ID: LCS 720-17537/2-AA Analysis Batch: 720-17745 Instrument ID: HP DRO5 <br /> Client Matrix: Solid Prep Batch. 720-17537 Lab File ID: N/A <br /> Dilution: 1.0 Units: mg/Kg Initial Weight/Volume. 30.43 g <br /> Date Analyzed: 01/24/2007 1746 Final Weight/Volume: 5 mL <br /> Date Prepared: 01/24/2007 1348 Injection Volume: <br /> Column ID: PRIMARY <br /> LCSD Lab Sample ID:LCSD 720-17537/3-AA Analysis Batch: 720-17745 Instrument ID: HP DRO5 <br /> Client Matrix: Solid Prep Batch: 720-17537 Lab File ID: N/A <br /> Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 30.15 g <br /> Date Analyzed: 01/24/2007 1813 Final Weight/Volume: 5 mL <br /> Date Prepared: 01/24/2007 1348 Injection Volume: <br /> Column ID: PRIMARY <br /> % Rec. <br /> Analyte LCS LCSD Limit RPD RPD Limit LCS Qua] LCSD Qual <br /> Diesel Range Organics[C9-C24] 84 84 50- 130 2 30 <br /> Surrogate LCS% Rec LCSD% Rec Acceptance Limits <br /> o-Terphenyl 79 79 50- 130 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Pacie 57 of 63 <br />