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Quality Control Results <br /> Client: SECOR International, Inc. Job Number: 720-7408-1 <br /> Method Blank -Batch: 720-17569 Method: 8015B <br /> Preparation: 3650B <br /> Lab Sample ID: MB 720-17569/1-AA Analysis Batch: 720-17634 Instrument ID: HP DR05 <br /> Client Matrix: Solid Prep Batch: 720-17569 Lab File ID: N/A <br /> Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 30.34 g <br /> Date Analyzed: 01/26/2007 1538 Final Weight/Volume: 5 mL <br /> Date Prepared: 01/25/2007 1207 Injection Volume: <br /> Column ID: PRIMARY <br /> Analyte Result Qual RL <br /> Diesel Range Organics[C9-C24] ND 0.99 <br /> Surrogate % Rec Acceptance Limits <br /> o-Terphenyl 77 50- 130 <br /> Lab Control Spike/ Method: 8015B <br /> Lab Control Spike Duplicate Recovery Report- Batch: 720-17569 Preparation: 3550B <br /> LCS Lab Sample ID: LCS 720-17569/2-AA Analysis Batch: 720-17634 Instrument ID: HP DR05 <br /> Client Matrix: Solid Prep Batch: 720-17569 Lab File ID: N/A <br /> Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 30.39 g <br /> Date Analyzed: 01/26/2007 1626 Final Weight/Volume: 5 mL <br /> Date Prepared: 01/25/2007 1207 Injection Volume: <br /> Column ID: PRIMARY <br /> LCSD Lab Sample ID:LCSD 720-17569/3-AA Analysis Batch: 720-17634 Instrument ID: HP DR05 <br /> Client Matrix: Solid Prep Batch: 720-17569 Lab File ID: N/A <br /> Dilution: 1.0 Units: mg/Kg Initial Weight/Volume: 30.18 g <br /> Date Analyzed: 01/26/2007 1743 Final Weight/Volume: 5 mL <br /> Date Prepared: 01/25/2007 1207 Injection Volume: <br /> Column ID: PRIMARY <br /> % Rec. <br /> Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual <br /> Diesel Range Organics[C9-C24] 79 77 50-130 2 30 <br /> Surrogate LCS% Rec LCSD% Rec Acceptance Limits <br /> o-Terphenyl 80 77 50-130 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Pace 58 of 63 <br />