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Quality Control Results <br /> Client: SECOR International, Inc. Job Number: 720-7408-1 <br /> Matrix Spike/ Method: 8015B <br /> Matrix Spike Duplicate Recovery Report- Batch: 720-17569 Preparation: 3550B <br /> MS Lab Sample ID: 720-7419-A-1-D MS Analysis Batch: 720-17634 Instrument ID: HP DR05 <br /> Client Matrix: Solid Prep Batch: 720-17569 Lab File ID: N/A <br /> Dilution: 1.0 Initial Weight/Volume: 30.18 g <br /> Date Analyzed: 01/25/2007 2054 Final Weight/Volume: 5 mL <br /> Date Prepared: 01/25/2007 1207 Injection Volume: <br /> Column ID: PRIMARY <br /> MSD Lab Sample ID: 720-7419-A-1-E MSD Analysis Batch: 720-17634 Instrument ID: HP DR05 <br /> Client Matrix: Solid Prep Batch: 720-17569 Lab File ID: N/A <br /> Dilution: 1.0 Initial Weight/Volume: 30.28 g <br /> Date Analyzed: 01/25/2007 2122 Final Weight/Volume: 5 mL <br /> Date Prepared: 01/25/2007 1207 Injection Volume: <br /> Column ID: PRIMARY <br /> % Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qua[ MSD Qual <br /> Diesel Range Organics[C9-C24] 83 61 60-136 20 30 <br /> Surrogate_ MS%Rec MSD%Rec Acceptance Limits <br /> o-Terphenyl 77 83 50-130 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 59 of 63 <br />