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x , <br /> CASTLE ANALYTICAL LABORATORY EB U 6 Z017 <br /> Environmental <br /> Certificate#248pesting Services 2333 Shuffle Drive,AENVIRC 301 -N-TAL HEALTH CA Phone,(209)3114-2930 <br /> Fax:(209)384-1507 <br /> American Valley Waste Oil,Inc. Client Project ID:Farmington Fresh Sampled: 01-17-17 <br /> P.O.Box 340 Lab Reference Number: 1701037 Received: 01-18-17 <br /> Delhi,CA 95315 Sample Description:Soil Extracted: 01-23-17 <br /> Attn:Steve Meier Sample Prep/Analysis Method: EPA 5030/8260 Analyzed: 01-23-17 <br /> Lab Numbers:1701037-01 Reported: 01-25-17 <br /> Client Sample ID:FF151220 <br /> VOLATILE ORGANICS-EPA METHOD 8260 GC/MS <br /> REPORTING PQL SAMPLE REPORTING PQL SAMPLE <br /> ANALYTE LIMIT RESULT ANALYTE LIMIT RESULT <br /> m it m mlk m it (mg/kg) m /k <br /> Benzene 0.0050 0.0050 NO 1,1-Dichlompmpene 0.0050 0.0050 NO <br /> Bromobenzene 0.0050 0.0050 NO cis-1,3-Dichloro roene 0.0050 0.0050 NO <br /> Bromochloromethane 0.0050 0.0050 NO trans-l,3-Dichioro roene 0.0050 0.0050 NO <br /> Bromodichloromethane 0.0050 0.0050 NO Eth (benzene 0.0050 0.0050 NO <br /> Bromoform 0.0050 0.0050 NO Hexachlorobutadiene 0.0050 0.0050 NO <br /> Bromomethane 0.0050 0.0050 NO Isopropylbenzene 0.0050 0.0050 NO <br /> n-Butylbenzene 0.0050 1 0.0050 NO p-Isopropyltoluene 0.0050 0.0050 1 NO <br /> sec8 (benzene 0.0050 0.0050 NO Methylene chloride 0.010 0.010 NO <br /> tert-Butylbenzene 0.0050 0.0050 NO Naphthalene 0.010 0.010 NO <br /> Carbon tetrachloride 0.0050 0.0050 NO n-Propylbenzene 0.0050 0.0050 NO <br /> Chlorobenzene 0.0050 0.0050 NO Styrene 0.0050 0.0050 NO <br /> Chlorodibromomethane 0.0050 0.0050 NO 1,1,1,2-Tetrachloroethane 0.0050 0.0050 NO <br /> Chloroethane 0.0050 0.0050 NO 1,1,2,2,-Telrachlorethane 0.0050 0,0050 ND <br /> Chloroform 0.0050 0.0050 NO Tetrachlorcethene 0.0050 0.0050 NO <br /> Chloromethane 0.0050 0.0050 NO Toluene 0.0050 0.0050 NO <br /> 2-Chlorotoluene 0.0050 0.0050 1 NO 1,2,3-Trichlorobenzene 0.0050 0.0050 NO <br /> 4-Chlorotoluene 0.0050 0.0050 NO 1,2,4-Trichlorobenzene 0.0050 0.0050 NO <br /> 1 2-Dibromo-3-chloro ro ane 0.010 0.010 NO 1,1,1-Trichloroethane 0.0050 0.0050 NO <br /> 12-Dibromoethane EDB 0.0050 0.0050 ND 1,12-Trichloroethane 0.0050 0.0050 NO <br /> Dibromomethane 0.0050 0.0050 NO Trichloroethene 0.0050 0.0050 NO <br /> 1,2-Dichlorobenzene 0.0050 0.0060 NO Trichlorofluoromethane 0.0050 0.0050 NO <br /> 1,3-Dichlorobenzene 0.0050 0.0050 NO 1,2,3-Trichloro ro ane 0.0050 0.0050 NO <br /> 1,4-Dichlorobenzene 0.0050 0.0050 NO 1 2,4-Trimeth (benzene 0.0050 0.0050 NO <br /> Dichlorodifluoromethane 0.0050 0.0050 NO 1,3,5-Trimeth (benzene 0.0050 0.0050 NO <br /> 1,1-Dichloroethane 0.0050 0.0050 NO Vinyl Chloride 0.0050 0.0050 NO <br /> 1,2-Dichloroethane 1,2-DCA 0.0050 0.0050 NO Xylenes,total 0.0050 0.0050 NO <br /> 1,1-Dichloroethene 0.0050 0.0050 ND Oxygenates <br /> cis-1,2-Dlchloroethene 0.0050 0.0050 ND tert-Butyl Alcohol(tBA) 0.10 0.10 1 NO <br /> trans-1,2-Dichloroethene 0.0050 0.0050 ND Methyl tert-Bu (Ether MTBE 0.0050 0.0050 ND <br /> 1,2-Dichloro ro ane 0.0050 0.0050 ND Di-Isopropyl Ether DIPE 0.0050 0.0050 NO <br /> 1,3-Dichloro ro ane 0.0050 0.0050 ND Ethyl tert-Bulyl Ether EtBE 0.0050 0.0050 NO <br /> 2,2-Dichloro ro ne 0.0050 0.0050 ND tert-Am I Methy Ether LAME 0.0050 0.0050 NO <br /> Surrogate Recoveries <br /> Dibromofluoromethane 103% Toluene-d8 87.5% <br /> 1,2-Dichloroethane-d4 104% p-Bromofluorobenzene 91.2% <br /> Instrument ID:VARIAN MS <br /> Analytes reported as NO were not detected or below the Practical quantitation Limit. <br /> Practical Quantitation Limit(PQL)=Reporting Limit x Dilution Factor <br /> (mg/kg)= milligrams per kilogram or parts per million(ppm) <br /> APPROVED BY: lz'dd LIZ <br /> James C.Phillip /Laboratory Director or <br /> Clan J. Cone/ borstory Manager <br />