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RE <br /> FEB 0 6 2017 <br /> CASTLE ANALYTICAL LABORATORY T, <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater,CA 95301 _ hone: (209)384-2930 <br /> Certificate#2480 - "T Fax: (209)384-1507 <br /> American Valley Waste Oil, Inc. Client Project ID:Farmington Fresh Method: EPA 5030/82608 <br /> P.O. Box 340 Lab Reference Number:1701037 Instrument ID:VARIAN MS <br /> Delhi,CA 95315 Sample Description:Soil Prepared: 01-23-17 <br /> Attn:Steve Meier Analyzed: 01-23-17 <br /> Reported: 01-25-17 <br /> QUALITY CONTROL DATA REPORT <br /> SPIKE ID: VSMS-1237 DP <br /> Reporting BLANK Spiking Control %R <br /> Limit Result Level Spike Limits <br /> ma/K ma/K mg/Kg %R <br /> COMPOUNDS <br /> t-ButylAlcohol(t-BA) 0.10 NO 3.0 97.3% 70.130 <br /> Methyl t-bLtyl ether MTBE 0.0050 NO 0.10 95.6% 70.130 <br /> Diiso ro I ether DIPE 0.0050 ND 0.10 102% 70-130 <br /> Ethyl t-Butyl ether ETBE 0.0050 NO 0.10 96.8% 70-130 <br /> t-Am 1 methyl ether TAME 0.0050 NO 0.10 95.2% 70-130 <br /> 1,2-Dichloroethane 1,2-DCA 0.0050 NO 1 0.10 91.2% 70-130 <br /> Ethylene dibromide EDB 0.0050 NO 0.10 93.6% 70-130 <br /> 1,1-Dichloroethene 1,1,DCE 0.0050 NO 0.10 96.0% 70-130 <br /> Benzene 0.0050 NO 0.10 93.6% 70-130 <br /> Trichloroethene(TCE) 0.0050 NO 0.10 95.6% 70-130 <br /> Toluene 0.0050 ND 0.10 92.4% 70-130 <br /> Chlorobenzene 0.0050 NO 0.10 92.8% 70.130 <br /> Surrogate: <br /> Dibromofluoromethane 0.10 103% 0.4098.4% 7070-130 <br /> 1,2-Dichloroethane-d4 0.10 98.8% 0.40 95.6% -130 <br /> Toluene-d8 0.10 103% 0.40 1 97.9% 70-130 <br /> 4-Bromofluorobenzene 0.10 115% 0.40 1 97.0% 70-130 <br /> Spiking MATRIX MATRIX %R %RPD <br /> Level SPIKE SPIKE OUP Limits <br /> ma/K %R %R <br /> COMPOUNDS <br /> t-ButylAlcohol(t-BA) 3.0 130% 169% 60-130% 26.1% <br /> Methyl t-butyl ether MTBE 0.10 99.2% 112% 70-130% 11.9% <br /> Diiso ro I ether DIPE 0.10 108% 112% 70-130% 2.37% <br /> Ethyl t-Butyl ether ETBE 0.10 100% 107% 70-130% 6.36% <br /> t-Am I methyl ether TAME 0.10 95.6% 100% 70.130% 4.50% <br /> 1,2-Dichloroethane 1,2-DCA 0.10 96.8% 107% 70-130% 9.85% <br /> Ethylene ibromide EDB 0.10 84.8% 91.2% 70.130% 7.27% <br /> 1,1-Dichloroethene 1,1,DCE 0.10 106% 96.8% 60.130% 9.07% <br /> Benzene 0.10 94.0% 87.6% 70-130% 6.81% <br /> Trichloroethene CE 0.10 83.6% 73.6% 70-130% 12.7% <br /> Toluene 0.10 77.2% 72.8% 70-130% 5.71% <br /> Chlorobenzene 0.10 94.8% 90.4% 70-130% 4.75% <br /> Surrogate: <br /> Dibromofluoromethane 0.40 104% 111% 70-130% 6.54% <br /> 1,2-Dichloroethane-d4 0.40 106% 119% 70.130% 11.2% <br /> Toluene-d8 0.40 83.0% 77.6% 70-130% 6.72% <br /> 4-Bromofluorobenzene 0.40 79.2% 1 79.3% 70-130% 1 0.126% <br /> APPROVED BY: <br /> James C. Phillip /Laboratory Director or <br /> Clan J. Cone/r <br /> boratory Manager <br />