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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL-ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.mccarnpbell.com E-mail: main@mccampbell.com <br /> • <br /> Advanced GeoEnvironmental Client Project ID: Shockey&Son Date Sampled: 04/11/01 <br /> 837 Shaw Road Date Received: 04/13/01 <br /> ' Stockton, CA 95215 Client Contact:Bill Little Date Extracted: 04/13/01 <br />' Client P.O: Date Analyzed: 04/13-04/19/01 <br /> Diesel Range(C10-C23)Extractable Hydrocarbons as Diesel * <br /> EPA methods modified 8015,and 3550 or 3510;California RWQCB(SF Bay Region)method GCFID(3550)or GCFID(3510) <br /> Lab ID Client ID Matrix TPH(d)+ %Recovery <br /> Surrogate <br /> 65422 MW1/04-11-01 W 6600,a 99 <br /> r65423 MW2/04-11-01 W 900,c,g 102 <br /> 65424 MW3/04-11-01 W 400,c 99 <br /> 65425 MW4/04-11-01 W 85,000,a,h 81 <br />' Reporting Limit unless otherwise W 50 ug/L. <br /> stated;ND means not detected above <br /> the reporting limit S 1.0 mg/kg <br /> *water and vapor samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP/STLC/SPLP <br /> extracts in ug/L <br /> -'cluttered chromatogram resulting in coeluted surrogate and sample peaks,or;'surrogate peak is on elevated baseline,or;surrogate has been - <br /> diminished by dilution of original extract. <br />' "Che following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation:a)unmodified or weakly modified diesel is significant;b)diesel range compounds are significant;no recognizable pattern;c) <br /> • aged diesel?is significant);d)gasoline range compounds are significant;e)medium boiling point pattern that does not match diesel(?); t) <br /> one to a few isolated peaks present; g) oil range compounds are significant; h) lighter than water immiscible sheen is present; i) liquid <br /> sample that contains greater than—5 vol.%sediment. <br />' DHS Certification No. 1644 Edward Hamilton,Lab Director <br />