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j' <br /> 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br />' MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622- <br /> htty://www.mccampbell.com E-mail: main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Shockey& Son Date,Sampled: 04/11/O1 <br /> 837 Shaw Road Date Received:04/13/01 <br /> Stockton, CA 95215 Client Contact: Bill Little Date Extracted: 04/19/01 <br />' Client P.O: Date Analyzed:04/19/01 <br /> Seven Oxygenated Volatile Organics By GUMS <br /> EPA method 8260 modified <br />' Lab ID 65422 65423 65424 65425 <br /> MWI/ MW2/ MW3/ MW4/ Reporting Limit <br /> Client ID 04-11-01 04-11-01 04-11-01 04-11-01 <br />' Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DIPE) ND ND ND ND 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETRE) ND ND ND ND 5.0 1.0 <br />' Methyl tert-Butyl Ether(MTBE) ND ND ND 3.1 5.0 1.0 <br /> ten-Amyl Methyl Ether(TAME) ND ND ND ND 5.0 1.0 <br />' tert-Butanol ND ND ND ND 25 5.0 <br /> Methanol ND ND ND ND 1000 500 <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries(%} <br />' Dibromofluoromethane 107 92 92 91 <br />' Comments- h <br />' *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC 1 SPLP extracts in ug/L <br /> _•= -_= -- ND means not detected above the reporting limit;NIA means surrogate not applicable to this analysis - <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than-5 vol,%sediment;(j)sample diluted due to <br />' high organic content <br />' DHS Certification No. 1644Edward Hamilton, Lab Director <br />