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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax :925-798-1622 <br /> ' http;//www.mccampbell.com E-mail:main@mccampbell.com <br /> ' Advanced GeoEnvironmental Client Project ID: Shockey&Son's Date Sampled:07/29/99 <br /> 4005 North Wilson Way Date Received:07/30/99 <br /> ' Stockton, CA 95205 Client Contact: Bill Little Date Extracted:07/30/99 <br /> ' Client P.O: Date Analyzed: 07130-08/03/99 <br /> Gasoline Range(C6-C]2)Volatile Hydrocarbons as Gasoline*,with Methyl tert-Butyl Ether*& BTEX* <br /> EPA methods 5030,modified 8015.and 8020 or 602:California RW CB(SF Ba Re ion)method GCFID 5030 <br /> (€)' Ethylben %Recovery <br /> Lab 1D Client ID Matrix TPH MTBE Benzene Toluene -zene Xylenes Surrogate <br /> 16359 P6-H20 W ND ND ND ND ND ND 104 <br /> ' 16360 P7-H20 W ND,i ND ND ND ND ND 108 <br /> 16361 P8-H20 W ND ND ND . ND ND ND 106 <br /> ' 16362 P9-H20 W NDJ ND ND ND ND ND 108 <br /> ' 16363 P11-H2OW NDJ ND ND ND ND ND 107 <br /> 16365 Pio-15 S 160,8 ND<0.10 ND ND ND ND 101 <br /> '• 16366 P10-20 S J 350_g ND<0.40 ND<0.02 ND<0,02 ND ND 101 <br /> 16367 P 10-25 S fi 14.g ND ND ND ND ND 99 <br />' 16368 P10-30 S I ND ND ND ND ND ND 95 <br /> 16369 P10-35 S ND ND ND ND ND ND 97 <br /> I <br /> 1 <br /> t <br /> Reporting Limit unle <br /> otherwie stated;ND Wj 50 ug/L 5.0 0.5 0.5 0.5 0.5 <br />' means not detected above <br /> the reporting limit S 1.0 mg/kg 0.05 0.005 0.00500 <br /> 0. 0.005 <br /> water and vapor samples are repotted in ug/L.wipe samples in ug/w-ipe,soil and sludge samples in mglkg,and all TCLP and SPLP extracts <br /> in ug/L <br /> 'cluttered chromatogram;sample peak:oelutes wiih surrogate peak <br /> 'The following descriptions of the I I'll chromatogram are cursory in nature and McCampbe]] Analytical is not responsible for their <br />' interpretation: a) unmodified or wCAIN modified gasoline is significant; b) heavier gasoline range compounds are signi6cant(aged <br /> gasoline?), 0 lighter gasohne rami <onipounds (1he most mobile fraction) are significant; d) gasoline range compounds having broad <br /> chromatographic peaks are sianificani. hiologicalh altered gasoline?:e)TPH pattern that does not appear to be derived from gasoline(?); f) <br /> one to a few isolated peaks present. i strongly aged gasoline or diesel range compounds arc significant; h)lighter than water immiscible <br /> sheen is resent;i li uid,;tm [e that c;mains ereaier than—5 vol.%sediment;")no reco nizab]e pattern. <br /> DHS Certification No. 1644 h Edward Hamilton, Lab Director <br />