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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> htt ://www.mccampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Shockey& Son's Date Sampled: 07/29/99 <br /> 4005 North Wilson Way Date Received: 07/30/99 <br /> Stockton,CA 95205 Client Contact: Bill Little Date Extractea:07/30/99 <br /> ' Client P.O: Date Analyzed: 07130-081106199 <br /> Diesel Range(CIO-C23)Extractable Hydrocarbons as Diesel * <br /> EPA methods modified 8015,and 33 1 or 3511,California RW CB(SF Bay Region)method GCFID 3550 or GCFID 3510 <br /> Lab ID Client ID Matrix TPH(d)` %Recovery <br /> Surrogate <br /> ' 16359 P6-H,0 W 850,g 105 <br /> 16360 P7-1-1 O W l 100,g,i 117 <br /> ' 16361 P8-H2O W ND 115 <br /> 16362 P9-H2O W NDJ 104 <br />' 16363 P11-H2O W 430,g,i 98 <br /> 16365 PIO-15 S 5100,a 109 <br /> lie 16366 PIG-20 S 13.000.a 99 <br /> 16367 P10-25 S 490,a 103 <br />' 16368 PIO-30 S ND 98 <br />' 16369 P10-35 S ND 100 <br /> I <br /> I <br /> 1 <br /> Reporting Limit unless otherwise W 50 ug/L <br />' stated;ND means not detected abo\c <br /> the reporting limit S 1.0 mg/kg <br /> I <br /> *water and vapor samples are reported in ug/L,a ipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP/STLC 1 SPLP <br />' extracts in ug/L. -- <br /> "cluttered chromatogram resulting in rceluted surrogate and sample peaks,or;surrogate peak is on elevated baseline,or;surrogate has been <br /> diminished by dilution of original <br />' "The following descriptions of the TPH chromawgram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation:a)unmodified or weak I\ modified diesel is significant;b)diesel range compounds are significant;no recognizable pattern;c) <br /> <aVd diesel?is significant);d)gasoline ranee compounds are significant;c)medium boiling point pattern that does not match diesel (?);f) <br />' one to a few isolated peaks present p oil range compounds are significant; h) lighter than water immiscible sheen is present; i) liquid <br /> sam le that contains nater than N of sediment. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br /> 1 <br />