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1 <br /> 110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br />' McCAMPBELL ANALYTICAL INC. Telephone :925-798-1620 Fax : 925-798-1622 <br /> h=://www.mccamnbell.com E-mail:main@mccampbell.com <br /> 1 Advanced GeoEnvironmental Client Project ID: Shockey& Son's Date Sampled: 07/29/99 <br /> 4005 North Wilson Way Date Received: 07/30/99 <br /> Stockton, CA 95205 Client Contact: Bill Little Date Extracted: 07/31/99 <br /> [Client <br /> P.O: Date Analyzed. 07131-08/05/99 <br />' Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 16359 16360 16361 16362 <br /> Reporting Limit <br /> Client ID P6-H2O P7-I-1,0 P8-H2O P9-H20 <br /> Matrix W W W W S W <br /> Compound Concentration' ug/kg ug/L <br />' Di-isopropyl Ether(DIPE) ND ND ND ND 5.0 1.0 <br /> Ethyl tent-Butyl Ether(ETRE) ND ND ND ND 5.0 1.0 <br /> Methyl-tert Buty]Ether(MTBE) ND ND ND ND 5.0 1.0 <br /> ten-Amyl Methyl Ether(TAME) ND ND ND ND 5.0 1.0 <br /> 1 tert-Butanol ND ND NDND 25 5.0 <br />' Surrogate Recoveries(%) <br /> Dibromofluoromethane 103 105 105 103 <br />' Comments: <br /> * water samples are reported in uJL.soil and sludge samples in ug/kg;wipes in ug/wipe and all TCLP I STLC I SPLP extracts in ug1L <br />' ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.".sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br /> 1 <br />