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1 GeoAnal tical Laboratories Inc. <br /> Y • <br /> 1405 Kansas Avenue Modesto,CA 95351 Phone (209)572-0900 Fax (209)572-0916 <br /> ' eport# M351-13 CERTIFICATE OF ANALYSIS Date: 12/28/01 <br /> (HF Environmental Date Rec'd: 12/17/01 <br /> ' Date Started: 12/20/01 <br /> PO Box 427 Project: Eckert Cold Storage Quarterly Date Completed: 12/27/01 <br /> Oakdale CA 95361 <br /> Date Sampled: 12/17/01 <br /> PO# Time: 12:28pm <br /> ' Sample ID: MW 4 Sampler : R Azevedo(Geo) <br /> Lab ID: M312468 <br /> ' Method RL Anal to Results Units <br /> 8260B 0.3 Benzene ND µg/l, <br /> 0.3 Toluene ND <br /> ' 0.3 Ethyl Benzene 1.6 <br /> 0.6 Total Xylenes 3.2 <br /> 1.0 Methyl tert-butyl ether (MTBE) 9.7 <br /> 40 Ethanol ND <br /> 20 tert-Butanol ND <br /> 1.0 di-Isopropyl ether'(DIPE) ND <br /> 1.0 Ethyl tert-butyl ether (ETBE) ND <br /> ' 1.0 tent-Amyl methyl ether (TAME) ND <br /> 1.0 Ethylene dibromide (EDB) ND { <br /> 0.5 1,2-Dichloroethane (1,2-DCA) 12 <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery OC Limit% <br /> 1,2-Dichloroethane-d, 5.00 4.76 95.2 72-132 <br /> 2-Bromo-l-chloropropane 5.00 4.20 84.0 71-134 <br /> 4-Bromofluorobenzene 5.00 4.18 83.6 74-132 <br /> a�l Psi [� . <br /> ' Mario D'Onofrio Donna Keller <br /> Chemist Certification # 1157 Laboratory Director <br />